Diminution of migration of phthalic acid esters in tequila beverage by the year of production

"The presence of diethyl-phthalate (DEP), dibutyl-phthalate (DBP), butylbenzyl-phthalate (BBP), diethylhexyl-phthalate (DEHP) and diisononyl-phthalate (DINP) was determined in 295 tequila samples. They were grouped by age of maturation (white, aged, extra aged or ultra aged) and year of product...

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Detalles Bibliográficos
Autores: VICTOR EMMANUEL BALDERAS HERNANDEZ, JOSE TOMAS ORNELAS SALAS, Ana Paulina Barba de la Rosa, Antonio de León Rodríguez
Tipo de recurso: artículo
Estado:Versión enviada para evaluación y publicación
Fecha de publicación:2020
País:México
Institución:Instituto Potosino de Investigación Científica y Tecnológica
Repositorio:Repositorio Institucional del IPICYT
OAI Identifier:oai:ipicyt.repositorioinstitucional.mx:1010/2472
Acceso en línea:http://ipicyt.repositorioinstitucional.mx/jspui/handle/1010/2472
Access Level:acceso abierto
Palabra clave:info:eu-repo/classification/Autor/Alcoholic beverages
info:eu-repo/classification/Autor/Endocrine disruptor
info:eu-repo/classification/Autor/Phthalate
info:eu-repo/classification/Autor/Plasticizer
info:eu-repo/classification/Autor/Tequila
info:eu-repo/classification/Autor/Spirits
info:eu-repo/classification/cti/3
info:eu-repo/classification/cti/32
info:eu-repo/classification/cti/3212
Descripción
Sumario:"The presence of diethyl-phthalate (DEP), dibutyl-phthalate (DBP), butylbenzyl-phthalate (BBP), diethylhexyl-phthalate (DEHP) and diisononyl-phthalate (DINP) was determined in 295 tequila samples. They were grouped by age of maturation (white, aged, extra aged or ultra aged) and year of production (between 2013 and 2018). Gas Chromatography coupled with Mass Spectrometry was used for identification and quantification. The results showed that 65 samples (22% of the total) were phthalate free. DEP (0.13-0.27?mg/kg), BBP (0.05?2.91?mg/kg) and DINP (1.64?3.43?mg/kg) were detected in 11 (3.73%), 37 (12.54%) and 5 (1.69%) samples, respectively. But, these concentrations did not exceed the maximum permitted limits (MPL) of phthalates for alcoholic beverages. DBP (0.01?2.20?mg/kg) and DEHP (0.03?4.64?mg/kg) were detected in 96 (32.54%) and 224 (75.93%) samples, from them only 10 (3.39%) and 15 (5.08%) samples, respectively, exceeded the MPL for alcoholic beverages and they were few tequilas produced in the year 2014 or before. DEHP was the most frequent phthalate found in tequila and observed DEHP concentrations were 2-times higher in ultra aged tequilas compared to those in white tequilas. We concluded that all tequilas produced in 2015 and after, satisfied the international standards for these compounds."