Complexation of the non-steroidal anti-inflammatory drug Nabumetone with modified and unmodified cyclodextrins

[EN]The inclusion of the anti-inflammatory drug, Nabumetone, in α-, β-and hydroxypropylβ-cyclodextrin (CDs) is studied using UV-VIS absorption and steady-state fluorescence emission. Binding constants and thermodynamic parameters of complex formation are determined by spectrofluorimetry. The inclusi...

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Detalles Bibliográficos
Autores: Valero Juan, Margarita, Costa, S.M.B., Ascenso, José R., Velázquez Salicio, María Mercedes, Rodríguez Hernández, Licesio Jesús
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:1999
País:España
Institución:Universidad de Salamanca (USAL)
Repositorio:GREDOS. Repositorio Institucional de la Universidad de Salamanca
OAI Identifier:oai:dnet:gredos______::96ca134a5621589726214570eeec5e38
Acceso en línea:http://hdl.handle.net/10366/171051
Access Level:acceso abierto
Palabra clave:Nabumetone
Naproxen
Cyclodextrin
UV-absorption spectroscopy
Fluorescence spectroscopy
Thermodynamics
Proton NMR
Cyclodextrins
Spectrometry, Fluorescence
ciclodextrinas
espectrometría de fluorescencia
naproxeno
Descripción
Sumario:[EN]The inclusion of the anti-inflammatory drug, Nabumetone, in α-, β-and hydroxypropylβ-cyclodextrin (CDs) is studied using UV-VIS absorption and steady-state fluorescence emission. Binding constants and thermodynamic parameters of complex formation are determined by spectrofluorimetry. The inclusion phenomena of Nabumetone with the three cyclodextrins is compared with that of the well known similar anti-inflammatory drug Naproxen. In the case of Nabumetone pronounced differences are observed in the complexation process with each cyclodextrin whereas the respective Naproxen complexes are nearly identical. 1H-NMR experiments show that the inclusion process in Nabumetone can occur either through the substituents in the -2 (butanone) or -6 (methoxy) positions in the naphthalene ring.