Recent advances in solid phase extraction involving nanomaterials for analytical purpose: A critical view

One of the main objectives for analytical chemists is the accurate and precise determination of target analytes in real samples. Although solid-phase extraction (SPE) has been a traditional and standard approach to achieve this purpose, conventional sorbents often suffer from limited selectivity, po...

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Detalles Bibliográficos
Autores: Montoro Leal, Pablo, Zougagh, Mohammed, Ríos Castro, Ángel
Tipo de recurso: artículo
Fecha de publicación:2025
País:España
Institución:Universidad de Castilla-La Mancha
Repositorio:RUIdeRA. Repositorio Institucional de la UCLM
OAI Identifier:oai:ruidera.uclm.es:10578/47365
Acceso en línea:https://doi.org/10.1016/j.trac.2025.118643
https://hdl.handle.net/10578/47365
Access Level:acceso abierto
Palabra clave:Sample preparation
Nanomaterials
Analytical methodologies
Sorbent materials
Analytical applications
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spelling Recent advances in solid phase extraction involving nanomaterials for analytical purpose: A critical viewMontoro Leal, PabloZougagh, MohammedRíos Castro, ÁngelSample preparationNanomaterialsAnalytical methodologiesSorbent materialsAnalytical applicationsOne of the main objectives for analytical chemists is the accurate and precise determination of target analytes in real samples. Although solid-phase extraction (SPE) has been a traditional and standard approach to achieve this purpose, conventional sorbents often suffer from limited selectivity, poor regeneration capacity, and a narrow sorption range, which restrict their applicability in challenging analytical scenarios. In this context, nanomaterials emerged as promising alternatives because of their tunable composition and structure, functionalizable surface, high specific surface area, and remarkable thermal, chemical, and physical stability. Relevant literature related to their use as sorbents in sample preparation protocols published in 2020–2025 are discussed. The period of last five years has been selected since a marked increase in the development of advanced two-dimensional nanosorbents, hybrid nanocomposites, and novel sustainable approaches has been noted, consolidating previously observed trends in this field. This review focuses on used nanomaterials, extraction methodology, and applications, including target analytes, and real samples. Additionally, an evaluation of key drawbacks derived from the use of nanomaterials such as aggregation tendency, cost-effectiveness for routine applications, and regulatory concerns is addressed. Although the nanomaterials have already demonstrated the potential to overcome limitations of conventional SPE sorbents, their definitive implementation will depend on addressing these unresolved challenges. This work is intended to provide an update on this topic and underscore future research directions that may enable practical implementation of nanomaterials as sorbents.Elsevier202620262025info:eu-repo/semantics/articleapplication/pdfhttps://doi.org/10.1016/j.trac.2025.118643https://hdl.handle.net/10578/47365reponame:RUIdeRA. Repositorio Institucional de la UCLMinstname:Universidad de Castilla-La ManchaInglésPID2022-138761NB-100PCI2024-153413SBPLY/24/180225/0001622025-GRIN-38523info:eu-repo/semantics/openAccessAttribution-NonCommercial-NoDerivs 3.0 Spainhttp://creativecommons.org/licenses/by-nc-nd/3.0/es/oai:ruidera.uclm.es:10578/473652026-05-27T07:36:41Z
dc.title.none.fl_str_mv Recent advances in solid phase extraction involving nanomaterials for analytical purpose: A critical view
title Recent advances in solid phase extraction involving nanomaterials for analytical purpose: A critical view
spellingShingle Recent advances in solid phase extraction involving nanomaterials for analytical purpose: A critical view
Montoro Leal, Pablo
Sample preparation
Nanomaterials
Analytical methodologies
Sorbent materials
Analytical applications
title_short Recent advances in solid phase extraction involving nanomaterials for analytical purpose: A critical view
title_full Recent advances in solid phase extraction involving nanomaterials for analytical purpose: A critical view
title_fullStr Recent advances in solid phase extraction involving nanomaterials for analytical purpose: A critical view
title_full_unstemmed Recent advances in solid phase extraction involving nanomaterials for analytical purpose: A critical view
title_sort Recent advances in solid phase extraction involving nanomaterials for analytical purpose: A critical view
dc.creator.none.fl_str_mv Montoro Leal, Pablo
Zougagh, Mohammed
Ríos Castro, Ángel
author Montoro Leal, Pablo
author_facet Montoro Leal, Pablo
Zougagh, Mohammed
Ríos Castro, Ángel
author_role author
author2 Zougagh, Mohammed
Ríos Castro, Ángel
author2_role author
author
dc.subject.none.fl_str_mv Sample preparation
Nanomaterials
Analytical methodologies
Sorbent materials
Analytical applications
topic Sample preparation
Nanomaterials
Analytical methodologies
Sorbent materials
Analytical applications
description One of the main objectives for analytical chemists is the accurate and precise determination of target analytes in real samples. Although solid-phase extraction (SPE) has been a traditional and standard approach to achieve this purpose, conventional sorbents often suffer from limited selectivity, poor regeneration capacity, and a narrow sorption range, which restrict their applicability in challenging analytical scenarios. In this context, nanomaterials emerged as promising alternatives because of their tunable composition and structure, functionalizable surface, high specific surface area, and remarkable thermal, chemical, and physical stability. Relevant literature related to their use as sorbents in sample preparation protocols published in 2020–2025 are discussed. The period of last five years has been selected since a marked increase in the development of advanced two-dimensional nanosorbents, hybrid nanocomposites, and novel sustainable approaches has been noted, consolidating previously observed trends in this field. This review focuses on used nanomaterials, extraction methodology, and applications, including target analytes, and real samples. Additionally, an evaluation of key drawbacks derived from the use of nanomaterials such as aggregation tendency, cost-effectiveness for routine applications, and regulatory concerns is addressed. Although the nanomaterials have already demonstrated the potential to overcome limitations of conventional SPE sorbents, their definitive implementation will depend on addressing these unresolved challenges. This work is intended to provide an update on this topic and underscore future research directions that may enable practical implementation of nanomaterials as sorbents.
publishDate 2025
dc.date.none.fl_str_mv 2025
2026
2026
dc.type.none.fl_str_mv info:eu-repo/semantics/article
format article
dc.identifier.none.fl_str_mv https://doi.org/10.1016/j.trac.2025.118643
https://hdl.handle.net/10578/47365
url https://doi.org/10.1016/j.trac.2025.118643
https://hdl.handle.net/10578/47365
dc.language.none.fl_str_mv Inglés
language_invalid_str_mv Inglés
dc.relation.none.fl_str_mv PID2022-138761NB-100
PCI2024-153413
SBPLY/24/180225/000162
2025-GRIN-38523
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
Attribution-NonCommercial-NoDerivs 3.0 Spain
http://creativecommons.org/licenses/by-nc-nd/3.0/es/
eu_rights_str_mv openAccess
rights_invalid_str_mv Attribution-NonCommercial-NoDerivs 3.0 Spain
http://creativecommons.org/licenses/by-nc-nd/3.0/es/
dc.format.none.fl_str_mv application/pdf
dc.publisher.none.fl_str_mv Elsevier
publisher.none.fl_str_mv Elsevier
dc.source.none.fl_str_mv reponame:RUIdeRA. Repositorio Institucional de la UCLM
instname:Universidad de Castilla-La Mancha
instname_str Universidad de Castilla-La Mancha
reponame_str RUIdeRA. Repositorio Institucional de la UCLM
collection RUIdeRA. Repositorio Institucional de la UCLM
repository.name.fl_str_mv
repository.mail.fl_str_mv
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