Morphology effects in photoactive ZnO nanostructures: photooxidative activity of polar surfaces

A series of ZnO nanostructures with variable morphology were prepared by a microemulsion method and their structural, morphological, and electronic properties were investigated by a combined experimental and theoretical approach using microscopy (high resolution transmission electron microscopy) and...

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Detalles Bibliográficos
Autores: Iglesias-Juez, Ana, Viñes Solana, Francesc, Lamiel Garcia, Josep Oriol, Fernandez-Garcia, Marcos, Illas i Riera, Francesc
Tipo de recurso: artículo
Estado:Versión aceptada para publicación
Fecha de publicación:2015
País:España
Institución:Universidad de Barcelona
Repositorio:Dipòsit Digital de la UB
OAI Identifier:oai:diposit.ub.edu:2445/165985
Acceso en línea:https://hdl.handle.net/2445/165985
Access Level:acceso abierto
Palabra clave:Fotocatàlisi
Òxid de zinc
Teoria del funcional de densitat
Photocatalysis
Zinc oxide
Density functionals
Descripción
Sumario:A series of ZnO nanostructures with variable morphology were prepared by a microemulsion method and their structural, morphological, and electronic properties were investigated by a combined experimental and theoretical approach using microscopy (high resolution transmission electron microscopy) and spectroscopic (X-ray diffraction, Raman, and UV-visible) tools, together with density functional theory calculations. The present experimental and computational study provides a detailed insight into the relationship between surface-related physicochemical properties and the photochemical response of ZnO nanostructures. Specifically, the present results provide evidence that the light-triggered photochemical activity of ZnO nanostructures is related to the predominance of highly-active (polar) surfaces, in particular, the amount of Zn-terminated (0001) surfaces, rather than band gap sizes, carrier mobilities, and other variables usually mentioned in the literature. The computational results highlight the oxidative capability of polar surfaces, independently of the degree of hydration.