Comparison of High Performance Liquid Chromatography with Fluorescence Detector and with Tandem Mass Spectrometry methods for detection and quantification of Ochratoxin A in green and roasted coffee beans

Instituto Nacional de Metrologia, Qualidade e Tecnologia. Diretoria de Metrologia Cientifíca e Industrial. Divisão de Metrologia Química. Duque de Caxias, RJ, Brasil.

Detalles Bibliográficos
Autores: Bandeira, Raquel Duarte da Costa Cunha, Uekane, Thais Matsue, Cunha, Carolina Passos da, Rodrigues, Janaína Marques, Cruz, Marcus Henrique Campino de la, Godoy, Ronoel Luiz de Oliveira, Fioravante, Andreia de Lima
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2013
País:Brasil
Institución:Fundação Oswaldo Cruz (FIOCRUZ)
Repositorio:Repositório Institucional da FIOCRUZ (ARCA)
Idioma:inglés
OAI Identifier:oai:arca.fiocruz.br:icict/8625
Acceso en línea:https://arca.fiocruz.br/handle/icict/8625
http://dx.doi.org/10.1590/S1516-89132013000600004
Access Level:acceso abierto
Palabra clave:HPLC-FLD
LC-MS/MS
Green Coffee
Roasted Coffee
Ochratoxins
Cromatografia Líquida de Alta Pressão
Espectrometria de Massas
Café
Ocratoxinas
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dc.title.none.fl_str_mv Comparison of High Performance Liquid Chromatography with Fluorescence Detector and with Tandem Mass Spectrometry methods for detection and quantification of Ochratoxin A in green and roasted coffee beans
title Comparison of High Performance Liquid Chromatography with Fluorescence Detector and with Tandem Mass Spectrometry methods for detection and quantification of Ochratoxin A in green and roasted coffee beans
spellingShingle Comparison of High Performance Liquid Chromatography with Fluorescence Detector and with Tandem Mass Spectrometry methods for detection and quantification of Ochratoxin A in green and roasted coffee beans
Bandeira, Raquel Duarte da Costa Cunha
HPLC-FLD
LC-MS/MS
Green Coffee
Roasted Coffee
Ochratoxins
Cromatografia Líquida de Alta Pressão
Espectrometria de Massas
Café
Roasted Coffee
Ocratoxinas
title_short Comparison of High Performance Liquid Chromatography with Fluorescence Detector and with Tandem Mass Spectrometry methods for detection and quantification of Ochratoxin A in green and roasted coffee beans
title_full Comparison of High Performance Liquid Chromatography with Fluorescence Detector and with Tandem Mass Spectrometry methods for detection and quantification of Ochratoxin A in green and roasted coffee beans
title_fullStr Comparison of High Performance Liquid Chromatography with Fluorescence Detector and with Tandem Mass Spectrometry methods for detection and quantification of Ochratoxin A in green and roasted coffee beans
title_full_unstemmed Comparison of High Performance Liquid Chromatography with Fluorescence Detector and with Tandem Mass Spectrometry methods for detection and quantification of Ochratoxin A in green and roasted coffee beans
title_sort Comparison of High Performance Liquid Chromatography with Fluorescence Detector and with Tandem Mass Spectrometry methods for detection and quantification of Ochratoxin A in green and roasted coffee beans
dc.creator.none.fl_str_mv Bandeira, Raquel Duarte da Costa Cunha
Uekane, Thais Matsue
Cunha, Carolina Passos da
Rodrigues, Janaína Marques
Cruz, Marcus Henrique Campino de la
Godoy, Ronoel Luiz de Oliveira
Fioravante, Andreia de Lima
author Bandeira, Raquel Duarte da Costa Cunha
author_facet Bandeira, Raquel Duarte da Costa Cunha
Uekane, Thais Matsue
Cunha, Carolina Passos da
Rodrigues, Janaína Marques
Cruz, Marcus Henrique Campino de la
Godoy, Ronoel Luiz de Oliveira
Fioravante, Andreia de Lima
author_role author
author2 Uekane, Thais Matsue
Cunha, Carolina Passos da
Rodrigues, Janaína Marques
Cruz, Marcus Henrique Campino de la
Godoy, Ronoel Luiz de Oliveira
Fioravante, Andreia de Lima
author2_role author
author
author
author
author
author
dc.subject.en.none.fl_str_mv HPLC-FLD
LC-MS/MS
Green Coffee
Roasted Coffee
Ochratoxins
topic HPLC-FLD
LC-MS/MS
Green Coffee
Roasted Coffee
Ochratoxins
Cromatografia Líquida de Alta Pressão
Espectrometria de Massas
Café
Roasted Coffee
Ocratoxinas
dc.subject.decs.none.fl_str_mv Cromatografia Líquida de Alta Pressão
Espectrometria de Massas
Café
Roasted Coffee
Ocratoxinas
description Instituto Nacional de Metrologia, Qualidade e Tecnologia. Diretoria de Metrologia Cientifíca e Industrial. Divisão de Metrologia Química. Duque de Caxias, RJ, Brasil.
publishDate 2013
dc.date.issued.fl_str_mv 2013
dc.date.accessioned.fl_str_mv 2014-10-17T18:58:19Z
dc.date.available.fl_str_mv 2014-10-17T18:58:19Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
format article
status_str publishedVersion
dc.identifier.citation.fl_str_mv BANDEIRA, R. D. C. C. et al. Comparison of High Performance Liquid Chromatography with Fluorescence Detector and with Tandem Mass Spectrometry methods for detection and quantification of Ochratoxin A in green and roasted coffee beans. Brazilian Archives of Biological Technology, Curitiba, v. 56, n. 6, p. 911-920. nov./dez. 2013.
dc.identifier.uri.fl_str_mv https://arca.fiocruz.br/handle/icict/8625
dc.identifier.issn.none.fl_str_mv 1516-8913
dc.identifier.doi.none.fl_str_mv http://dx.doi.org/10.1590/S1516-89132013000600004
identifier_str_mv BANDEIRA, R. D. C. C. et al. Comparison of High Performance Liquid Chromatography with Fluorescence Detector and with Tandem Mass Spectrometry methods for detection and quantification of Ochratoxin A in green and roasted coffee beans. Brazilian Archives of Biological Technology, Curitiba, v. 56, n. 6, p. 911-920. nov./dez. 2013.
1516-8913
url https://arca.fiocruz.br/handle/icict/8625
http://dx.doi.org/10.1590/S1516-89132013000600004
dc.language.iso.fl_str_mv eng
language eng
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.publisher.none.fl_str_mv Instituto de Tecnologia do Paraná
publisher.none.fl_str_mv Instituto de Tecnologia do Paraná
dc.source.none.fl_str_mv reponame:Repositório Institucional da FIOCRUZ (ARCA)
instname:Fundação Oswaldo Cruz (FIOCRUZ)
instacron:FIOCRUZ
instname_str Fundação Oswaldo Cruz (FIOCRUZ)
instacron_str FIOCRUZ
institution FIOCRUZ
reponame_str Repositório Institucional da FIOCRUZ (ARCA)
collection Repositório Institucional da FIOCRUZ (ARCA)
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spelling 2014-10-17T18:58:19Z2014-10-17T18:58:19Z2013BANDEIRA, R. D. C. C. et al. Comparison of High Performance Liquid Chromatography with Fluorescence Detector and with Tandem Mass Spectrometry methods for detection and quantification of Ochratoxin A in green and roasted coffee beans. Brazilian Archives of Biological Technology, Curitiba, v. 56, n. 6, p. 911-920. nov./dez. 2013.1516-8913https://arca.fiocruz.br/handle/icict/8625http://dx.doi.org/10.1590/S1516-89132013000600004engInstituto de Tecnologia do ParanáComparison of High Performance Liquid Chromatography with Fluorescence Detector and with Tandem Mass Spectrometry methods for detection and quantification of Ochratoxin A in green and roasted coffee beansinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articleInstituto Nacional de Metrologia, Qualidade e Tecnologia. Diretoria de Metrologia Cientifíca e Industrial. Divisão de Metrologia Química. Duque de Caxias, RJ, Brasil.Instituto Nacional de Metrologia, Qualidade e Tecnologia. Diretoria de Metrologia Cientifíca e Industrial. Divisão de Metrologia Química. Duque de Caxias, RJ, Brasil.Instituto Nacional de Metrologia, Qualidade e Tecnologia. Diretoria de Metrologia Cientifíca e Industrial. Divisão de Metrologia Química. Duque de Caxias, RJ, Brasil.Instituto Nacional de Metrologia, Qualidade e Tecnologia. Diretoria de Metrologia Cientifíca e Industrial. Divisão de Metrologia Química. Duque de Caxias, RJ, Brasil.Fundação Oswaldo Cruz. Instituto Nacional de Controle de Qualidade em Saúde. Comissão do Programa de Ensaio de Proficiência de Produtos Sujeitos ao Regime de Vigilância Sanitária. Rio de Janeiro, RJ, Brasil.Embrapa Agroindustria de Alimentos. Rio de Janeiro, RJ, Brasil.Instituto Nacional de Metrologia, Qualidade e Tecnologia. Diretoria de Metrologia Cientifíca e Industrial. Divisão de Metrologia Química. Duque de Caxias, RJ, Brasil.Two analytical methods for the determination and confirmation of ochratoxin A (OTA) in green and roasted coffee samples were compared. Sample extraction and clean-up were based on liquid–liquid phase extraction and immunoaffinity column. The detection of OTA was carried out with the high performance liquid chromatography (HPLC) combined either with fluorescence detection (FLD), or positive electrospray ionization (ESI+) coupled with tandem mass spectrometry (MS–MS). The results obtained with the LC-ESI-MS/MS were specific and more sensitive, with the advantages in terms of unambiguous analyte identification, when compared with the HPLC-FLD.HPLC-FLDLC-MS/MSGreen CoffeeRoasted CoffeeOchratoxinsCromatografia Líquida de Alta PressãoEspectrometria de MassasCaféRoasted CoffeeOcratoxinasinfo:eu-repo/semantics/openAccessreponame:Repositório Institucional da FIOCRUZ (ARCA)instname:Fundação Oswaldo Cruz (FIOCRUZ)instacron:FIOCRUZBandeira, Raquel Duarte da Costa CunhaUekane, Thais MatsueCunha, Carolina Passos daRodrigues, Janaína MarquesCruz, Marcus Henrique Campino de laGodoy, Ronoel Luiz de OliveiraFioravante, Andreia de LimaLICENSElicense.txtlicense.txttext/plain; charset=utf-81914https://arca.fiocruz.br/bitstreams/a9141e28-5fab-48e2-9402-72a0b139a25d/download7d48279ffeed55da8dfe2f8e81f3b81fMD51falseAnonymousREADORIGINALBraz Arch Biol Technol_56_911-920.pdfBraz Arch Biol Technol_56_911-920.pdfapplication/pdf222047https://arca.fiocruz.br/bitstreams/657af49a-f54c-4b91-9995-8ac2b98ebddb/download7812cf22f62960742e5b058d4f6a1274MD52trueAnonymousREADTEXTBraz Arch Biol Technol_56_911-920.pdf.txtBraz Arch Biol Technol_56_911-920.pdf.txtExtracted texttext/plain38734https://arca.fiocruz.br/bitstreams/e58d59fb-430a-4065-a382-77c8f14994c4/download0ae5a8c36c04e8820fcf5a5bfae1c3cbMD57falseAnonymousREADTHUMBNAILBraz Arch Biol Technol_56_911-920.pdf.jpgBraz Arch Biol Technol_56_911-920.pdf.jpgGenerated Thumbnailimage/jpeg42542https://arca.fiocruz.br/bitstreams/94276cae-12ea-41b5-873f-dca3cbbbe1d0/download6919fb38fcbe739577ba91a8b91def34MD58falseAnonymousREADicict/86252025-12-10 13:14:26.743open.accessoai:arca.fiocruz.br:icict/8625https://arca.fiocruz.brRepositório InstitucionalPUBhttps://www.arca.fiocruz.br/oai/requestrepositorio.arca@fiocruz.bropendoar:21352025-12-10T16:14:26Repositório Institucional da FIOCRUZ (ARCA) - Fundação Oswaldo Cruz (FIOCRUZ)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