Electro-Oxidation of Methanol on Pt-Ru Nanostructured Catalysts Electrodeposited onto Electroactivated Carbon Fiber Materials

The surface of different carbon substrates, such as glassy carbon (GC), graphite cloth (GC-10), graphite felt (GF-S2), and carbon fiber paper (CFP) was modified by electrochemical treatment to generate high concentrations of oxygenated functional groups. These activated carbons were used as substrat...

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Detalhes bibliográficos
Autores: Sieben, Juan Manuel, Duarte, Marta María Elena, Mayer, Carlos Enrique
Formato: artículo
Estado:Versión publicada
Fecha de publicación:2010
País:Argentina
Recursos:Consejo Nacional de Investigaciones Científicas y Técnicas
Repositorio:CONICET Digital (CONICET)
Idioma:inglés
OAI Identifier:oai:ri.conicet.gov.ar:11336/62002
Acesso em linha:http://hdl.handle.net/11336/62002
Access Level:acceso abierto
Palavra-chave:Carbon
Electrocatalysis
Oxidation
Platinum
Ruthenium
https://purl.org/becyt/ford/2.5
https://purl.org/becyt/ford/2
https://purl.org/becyt/ford/2.4
https://purl.org/becyt/ford/1.4
https://purl.org/becyt/ford/1
Descrição
Resumo:The surface of different carbon substrates, such as glassy carbon (GC), graphite cloth (GC-10), graphite felt (GF-S2), and carbon fiber paper (CFP) was modified by electrochemical treatment to generate high concentrations of oxygenated functional groups. These activated carbons were used as substrates for the simultaneous electrodeposition of Pt and Ru by a double potentiostatic pulse program. The different catalyst/carbon systems were evaluated as electrodes for methanol oxidation in acid solution. Comparing the results for the oxidized and nonoxidized substrates, the oxidation of the different carbon materials prior to the catalyst deposition was found to lead to an increase in the electrode activity for methanol oxidation. This enhancement could be associated with a remarkable improvement of metal dispersion, reduction of particle size, and a higher active surface area of the catalyst. The electrodes prepared with oxidized graphite felt exhibited the greatest catalytic activity. © 2010 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.