Pt-Ru polymeric electrocatalysts used for the determination of carbon monoxide

Different PtRu polyaniline composite catalysts were studied for the electro-oxidation of carbon monoxide (CO) in order to ascertain their response to the changes in CO bulk concentration in acid solutions. The catalyst substrate consisted of polyaniline films with incorporated carbon nanotubes grown...

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Detalles Bibliográficos
Autores: Bavio, Marcela Alejandra, Kessler, Teresita, Castro Luna Berenguer, Ana Maria del Carmen
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2012
País:Argentina
Institución:Consejo Nacional de Investigaciones Científicas y Técnicas
Repositorio:CONICET Digital (CONICET)
Idioma:inglés
OAI Identifier:oai:ri.conicet.gov.ar:11336/33294
Acceso en línea:http://hdl.handle.net/11336/33294
Access Level:acceso abierto
Palabra clave:Polimeric Electrodes
Platinum-Ruthenium
Carbon Monoxide
https://purl.org/becyt/ford/1.4
https://purl.org/becyt/ford/1
Descripción
Sumario:Different PtRu polyaniline composite catalysts were studied for the electro-oxidation of carbon monoxide (CO) in order to ascertain their response to the changes in CO bulk concentration in acid solutions. The catalyst substrate consisted of polyaniline films with incorporated carbon nanotubes grown over a Ni wire. To build the electrode, PtRu particles were added to the polymeric film by immersion at open circuit from a solution containing Pt(IV) and Ru(III). The concentration relationship R = [Pt(IV)]/[Ru(III)] was established fixing the Pt(IV) concentration and varying Ru(III) concentration in order to have 0.5 < R < 5. CO electro-oxidation in acid media was studied applying cyclic voltammetry and chronoamperometry, carefully controlling the amount of CO that flowed into the cell. A linear relationship was established between the CO oxidation current density and its concentration in solution for the catalyst prepared with lower R.