Improved Stability of Human CGI-58 Induced by Phosphomimetic S237E Mutation

"In lipolysis, the activating function of CGI-58 is regulated by its interaction with perilipin 1 (PLIN1) localized on the lipid droplet (LD), and its release is controlled by phosphorylation. Once lipolysis is stimulated by catecholamines, protein kinase A (PKA)-mediated phosphorylation enable...

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Detalles Bibliográficos
Autores: MIRIAM LIVIER LLAMAS GARCIA, Edgar Daniel Páez Pérez, CLAUDIA GUADALUPE BENITEZ CARDOZA, GABRIELA MARGARITA MONTERO MORAN, SAMUEL LARA GONZALEZ
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2022
País:México
Institución:Instituto Potosino de Investigación Científica y Tecnológica
Repositorio:Repositorio Institucional del IPICYT
OAI Identifier:oai:ipicyt.repositorioinstitucional.mx:1010/2583
Acceso en línea:http://ipicyt.repositorioinstitucional.mx/jspui/handle/1010/2583
Access Level:acceso abierto
Palabra clave:info:eu-repo/classification/Autor/Adipose triglyceride lipase
info:eu-repo/classification/Autor/Protein
info:eu-repo/classification/Autor/Binding
info:eu-repo/classification/Autor/Domain
info:eu-repo/classification/Autor/Solubility
info:eu-repo/classification/Autor/Prediction
info:eu-repo/classification/Autor/Lipolysis
info:eu-repo/classification/cti/2
info:eu-repo/classification/cti/23
Descripción
Sumario:"In lipolysis, the activating function of CGI-58 is regulated by its interaction with perilipin 1 (PLIN1) localized on the lipid droplet (LD), and its release is controlled by phosphorylation. Once lipolysis is stimulated by catecholamines, protein kinase A (PKA)-mediated phosphorylation enables the dissociation of the CGI-58/PLIN1 complex, thereby recruiting adipose triglyceride lipase (ATGL) and hormone-sensitive lipase (HSL) to initiate fatty acid release. It has been shown that mouse CGI-58 mutant S239E, which mimics the phosphorylation of this residue, is able to dissociate from the CGI-58/PLIN1 complex and activate ATGL. Here, we analyze the stabilizing effect on human CGI-58 of a triple tryptophan to alanine mutant (3WA) on the LD-binding motif, as well as a quadruple mutant in which the phosphomimetic S237E substitution was introduced to the 3WA construct (3WA/S237E). We found that tryptophan residues promote wild-type (WT) protein aggregation in solution since their substitution for alanine residues favors the presence of the monomer. Our experimental data showed increased thermal stability and solubility of 3WA/S237E protein compared to the 3WA mutant. Moreover, the 3WA/S237E protein showed proper folding and a functional binding site for oleoyl-CoA. The analysis of a bioinformatic three-dimensional (3D) model suggests an intramolecular interaction between the phosphomimetic glutamic acid and a residue of the α/β hydrolase core. This could explain the increased solubility and stability observed in the 3WA/S237E mutant and evidences the possible role of serine 237 phosphorylation."