STRUCTURAL DETERMINATION OF ε-LACTAMS BY 1H AND 13C NMR

The thermodynamic products (ε‐lactams) of the degradation of ten different spirocyclic oxaziridines were analyzed by 1H and 13C NMR spectroscopy. The preferred conformations were determined by examining the homonuclear spin–spin coupling constant and the chemical shift effects of the N‐substituent a...

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Detalhes bibliográficos
Autores: 123050, 123051, MONTALVO GONZALEZ, RUBEN, ARIZA CASTOLO, ARMANDO
Formato: artículo
Estado:Versión publicada
Fecha de publicación:2009
País:México
Recursos:Universidad Autónoma de Nayarit
Repositorio:Repositorio Institucional Aramara de la UAN
Idioma:inglés
OAI Identifier:oai:dspace.uan.mx:123456789/1972
Acesso em linha:https://doi.org/10.1002/mrc.2504
http://dspace.uan.mx:8080/jspui/handle/123456789/1972
Access Level:acceso abierto
Palavra-chave:RMN
1H
13C
conformación
e-lactámicas
conformation
e-lactams
MEDICINA Y CIENCIAS DE LA SALUD [3]
Descrição
Resumo:The thermodynamic products (ε‐lactams) of the degradation of ten different spirocyclic oxaziridines were analyzed by 1H and 13C NMR spectroscopy. The preferred conformations were determined by examining the homonuclear spin–spin coupling constant and the chemical shift effects of the N‐substituent and the alkyl group of the aliphatic ring on 1H and 13C NMR spectra.