Contribution of volatile compounds to the antioxidant capacity of coffee

Heterocyclic volatile compounds present in coffee have been proposed as potent antioxidants, but their contribution to the antioxidant capacity of coffee is still unclear and controversial. The aim of this study was to assess the actual contribution of the main volatile compounds to the overall anti...

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Autores: Ludwig-Sanz-Orrio, I.A. (Iziar Amaia)|||/items/6a2bbebb-4e48-4845-9e71-14638284ebb1, Sanchez, L. (Lidia)|||/items/58d5670d-97ee-462d-a831-1df611fbb205, Peña, M.P. (María Paz) de|||/items/573639ac-cfd4-4c83-ad42-32def0ce5522, Cid-Canda, C. (Concepción)|||/items/e0b35b0b-38b6-46f6-87fa-ee5cf58bf903
Tipo de recurso: artículo
Fecha de publicación:2014
País:España
Institución:Universidad de Navarra
Repositorio:Dadun. Depósito Académico Digital de la Universidad de Navarra
Idioma:inglés
OAI Identifier:oai:dadun.unav.edu:10171/36118
Acceso en línea:https://hdl.handle.net/10171/36118
Access Level:acceso abierto
Palabra clave:Antioxidants
Aroma
Coffee
GC/MS
Volatiles
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spelling Contribution of volatile compounds to the antioxidant capacity of coffeeLudwig-Sanz-Orrio, I.A. (Iziar Amaia)|||/items/6a2bbebb-4e48-4845-9e71-14638284ebb1Sanchez, L. (Lidia)|||/items/58d5670d-97ee-462d-a831-1df611fbb205Peña, M.P. (María Paz) de|||/items/573639ac-cfd4-4c83-ad42-32def0ce5522Cid-Canda, C. (Concepción)|||/items/e0b35b0b-38b6-46f6-87fa-ee5cf58bf903AntioxidantsAromaCoffeeGC/MSVolatilesHeterocyclic volatile compounds present in coffee have been proposed as potent antioxidants, but their contribution to the antioxidant capacity of coffee is still unclear and controversial. The aim of this study was to assess the actual contribution of the main volatile compounds to the overall antioxidant capacity of coffee. A total of sixty-two and sixty-four volatile compounds were identified and quantified in Arabica and Robusta coffee, respectively, by static headspace-gas chromatography-mass spectrometry (SH-GC-MS). ABTS (2,2′-Azino-bi(3-ethylbenzo-thiazonile-6-sulfonic acid) diammonium salt) and DPPH (2,2-Diphenyl-1-picrylhydrazyl) antioxidant activity of the most abundant volatile heterocyclic compounds (7 furans (Fu), 3 pyrroles (Py) and 2 thiophenes (Th)), aldehydes (5) and diketones (2) was evaluated in model systems at different concentrations including those found in coffee. The model system with all the heterocyclic volatiles (Fu–Py–Th) was the most active followed by pyrroles and furans. Thiophenes were ineffective as radical scavengers at all concentrations including 100-fold, and aldehydes and ketones showed negligible activities in comparison to heterocyclic volatiles. In addition, only furans exhibited linear concentration dependent ABTS antioxidant activity and individual volatile model systems showed that only 2-methyl-tetrahydrofuran-3-one and pyrrole for ABTS, and also 1-methylpyrrole for DPPH, were the main volatile compounds responsible for the coffee antioxidant activity. However, the contribution of the heterocyclic volatile compounds to the overall antioxidant capacity of a filter coffee brew was almost insignificant, even at 100-fold concentrated Fu–Py–Th model system, accounting only for up to 3.3%.ElsevierDadun. Depósito Académico Digital Universidad de Navarra20142014-07-0120142014-01-0120142014-01-01journal articlehttp://purl.org/coar/resource_type/c_6501info:eu-repo/semantics/articleapplication/pdfhttps://hdl.handle.net/10171/36118reponame:Dadun. Depósito Académico Digital de la Universidad de Navarrainstname:Universidad de NavarraInglésengopen accesshttp://purl.org/coar/access_right/c_abf2info:eu-repo/semantics/openAccessoai:dadun.unav.edu:10171/361182026-06-21T12:47:57Z
dc.title.none.fl_str_mv Contribution of volatile compounds to the antioxidant capacity of coffee
title Contribution of volatile compounds to the antioxidant capacity of coffee
spellingShingle Contribution of volatile compounds to the antioxidant capacity of coffee
Ludwig-Sanz-Orrio, I.A. (Iziar Amaia)|||/items/6a2bbebb-4e48-4845-9e71-14638284ebb1
Antioxidants
Aroma
Coffee
GC/MS
Volatiles
title_short Contribution of volatile compounds to the antioxidant capacity of coffee
title_full Contribution of volatile compounds to the antioxidant capacity of coffee
title_fullStr Contribution of volatile compounds to the antioxidant capacity of coffee
title_full_unstemmed Contribution of volatile compounds to the antioxidant capacity of coffee
title_sort Contribution of volatile compounds to the antioxidant capacity of coffee
dc.creator.none.fl_str_mv Ludwig-Sanz-Orrio, I.A. (Iziar Amaia)|||/items/6a2bbebb-4e48-4845-9e71-14638284ebb1
Sanchez, L. (Lidia)|||/items/58d5670d-97ee-462d-a831-1df611fbb205
Peña, M.P. (María Paz) de|||/items/573639ac-cfd4-4c83-ad42-32def0ce5522
Cid-Canda, C. (Concepción)|||/items/e0b35b0b-38b6-46f6-87fa-ee5cf58bf903
author Ludwig-Sanz-Orrio, I.A. (Iziar Amaia)|||/items/6a2bbebb-4e48-4845-9e71-14638284ebb1
author_facet Ludwig-Sanz-Orrio, I.A. (Iziar Amaia)|||/items/6a2bbebb-4e48-4845-9e71-14638284ebb1
Sanchez, L. (Lidia)|||/items/58d5670d-97ee-462d-a831-1df611fbb205
Peña, M.P. (María Paz) de|||/items/573639ac-cfd4-4c83-ad42-32def0ce5522
Cid-Canda, C. (Concepción)|||/items/e0b35b0b-38b6-46f6-87fa-ee5cf58bf903
author_role author
author2 Sanchez, L. (Lidia)|||/items/58d5670d-97ee-462d-a831-1df611fbb205
Peña, M.P. (María Paz) de|||/items/573639ac-cfd4-4c83-ad42-32def0ce5522
Cid-Canda, C. (Concepción)|||/items/e0b35b0b-38b6-46f6-87fa-ee5cf58bf903
author2_role author
author
author
dc.contributor.none.fl_str_mv Dadun. Depósito Académico Digital Universidad de Navarra
dc.subject.none.fl_str_mv Antioxidants
Aroma
Coffee
GC/MS
Volatiles
topic Antioxidants
Aroma
Coffee
GC/MS
Volatiles
description Heterocyclic volatile compounds present in coffee have been proposed as potent antioxidants, but their contribution to the antioxidant capacity of coffee is still unclear and controversial. The aim of this study was to assess the actual contribution of the main volatile compounds to the overall antioxidant capacity of coffee. A total of sixty-two and sixty-four volatile compounds were identified and quantified in Arabica and Robusta coffee, respectively, by static headspace-gas chromatography-mass spectrometry (SH-GC-MS). ABTS (2,2′-Azino-bi(3-ethylbenzo-thiazonile-6-sulfonic acid) diammonium salt) and DPPH (2,2-Diphenyl-1-picrylhydrazyl) antioxidant activity of the most abundant volatile heterocyclic compounds (7 furans (Fu), 3 pyrroles (Py) and 2 thiophenes (Th)), aldehydes (5) and diketones (2) was evaluated in model systems at different concentrations including those found in coffee. The model system with all the heterocyclic volatiles (Fu–Py–Th) was the most active followed by pyrroles and furans. Thiophenes were ineffective as radical scavengers at all concentrations including 100-fold, and aldehydes and ketones showed negligible activities in comparison to heterocyclic volatiles. In addition, only furans exhibited linear concentration dependent ABTS antioxidant activity and individual volatile model systems showed that only 2-methyl-tetrahydrofuran-3-one and pyrrole for ABTS, and also 1-methylpyrrole for DPPH, were the main volatile compounds responsible for the coffee antioxidant activity. However, the contribution of the heterocyclic volatile compounds to the overall antioxidant capacity of a filter coffee brew was almost insignificant, even at 100-fold concentrated Fu–Py–Th model system, accounting only for up to 3.3%.
publishDate 2014
dc.date.none.fl_str_mv 2014
2014-07-01
2014
2014-01-01
2014
2014-01-01
dc.type.none.fl_str_mv journal article
http://purl.org/coar/resource_type/c_6501
dc.type.openaire.fl_str_mv info:eu-repo/semantics/article
format article
dc.identifier.none.fl_str_mv https://hdl.handle.net/10171/36118
url https://hdl.handle.net/10171/36118
dc.language.none.fl_str_mv Inglés
eng
language_invalid_str_mv Inglés
language eng
dc.rights.none.fl_str_mv open access
http://purl.org/coar/access_right/c_abf2
dc.rights.openaire.fl_str_mv info:eu-repo/semantics/openAccess
rights_invalid_str_mv open access
http://purl.org/coar/access_right/c_abf2
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
dc.publisher.none.fl_str_mv Elsevier
publisher.none.fl_str_mv Elsevier
dc.source.none.fl_str_mv reponame:Dadun. Depósito Académico Digital de la Universidad de Navarra
instname:Universidad de Navarra
instname_str Universidad de Navarra
reponame_str Dadun. Depósito Académico Digital de la Universidad de Navarra
collection Dadun. Depósito Académico Digital de la Universidad de Navarra
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repository.mail.fl_str_mv
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