Improved Performance of a Europium-based Metal-Organic Framework for Cyanosilylation of Demanding Ketones

Solvothermally promoted assembly of the multifunctional 3-amino-4-hydroxybenzoic acid ligand with the corresponding Eu salt gives rise to the formation of a porous metal-organic framework with the general formula {[EuL(OH)(HO)] ⋅ 5DMF} (1) that has been tested as heterogeneous catalyst for the cyano...

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Detalles Bibliográficos
Autores: Pérez, Juana M., Echenique-Errandonea, Estitxu, Rojas, Sara, Choquesillo-Lazarte, Duane, Seco, José M., López-Vargas, Mireya E., Rodríguez-Diéguez, Antonio, Fernández, Ignacio
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2022
País:España
Institución:Consejo Superior de Investigaciones Científicas (CSIC)
Repositorio:DIGITAL.CSIC. Repositorio Institucional del CSIC
OAI Identifier:oai:digital.csic.es:10261/356885
Acceso en línea:http://hdl.handle.net/10261/356885
Access Level:acceso abierto
Palabra clave:Cyanosilylation
Europium
Heterogeneous catalysis
Ketones
Metal-organic framework
Descripción
Sumario:Solvothermally promoted assembly of the multifunctional 3-amino-4-hydroxybenzoic acid ligand with the corresponding Eu salt gives rise to the formation of a porous metal-organic framework with the general formula {[EuL(OH)(HO)] ⋅ 5DMF} (1) that has been tested as heterogeneous catalyst for the cyanosilylation of a broad scope of ketones in solvent-free conditions, using the lowest catalyst loading of 0.5 mol% ever reported, and exhibiting no leak and high recyclability.