Effects of Processing Conditions of a Ball-Milled Fe65Co35 Soft Ferromagnetic Alloy on the Structural, Thermal, and Magnetic Properties

The Fe65Co35 alloy is a well-known Fe-based soft ferromagnetic alloy with excellent soft magnetic properties, which make it a strong candidate to be used in technological applications. In the present work, synthesizing nanoscrystalline Fe65Co35 alloy by mechanical alloying is focused on, adding cycl...

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Detalles Bibliográficos
Autores: Daza Collier, Jason, Curbelo-Cano, Zaida, Montero, Cristina M., Ben Mbarek, Wael, Escoda i Acero, Ma. Lluïsa, Saurina Canals, Joan, Palmero, Ester M., Bollero, Alberto, Bruna, Pere, Suñol Martínez, Joan Josep
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2025
País:España
Institución:Varias* (Consorci de Biblioteques Universitáries de Catalunya, Centre de Serveis Científics i Acadèmics de Catalunya)
Repositorio:Recercat. Dipósit de la Recerca de Catalunya
OAI Identifier:oai:recercat.cat:10256/26862
Acceso en línea:http://hdl.handle.net/10256/26862
Access Level:acceso abierto
Palabra clave:Aliatges
Alloys
Aliatge mecànic
Mechanical alloying
Ferro -- Aliatges
Iron alloys
Ferromagnetisme
Ferromagnetism
Descripción
Sumario:The Fe65Co35 alloy is a well-known Fe-based soft ferromagnetic alloy with excellent soft magnetic properties, which make it a strong candidate to be used in technological applications. In the present work, synthesizing nanoscrystalline Fe65Co35 alloy by mechanical alloying is focused on, adding cyclohexane (C6H12) acting as a process control agent (PCA). PCAs are effective in favoring nanostructured alloys with uniform grain size. The production of this type of alloy is a promising approach to tune the magnetic hardness in Fe65Co35. Structural, thermal, morphological, and magnetic properties have been studied after milling for 10, 25, and 50 h with and without the PCA. In the structural analysis, it is shown that the cubic α-Fe(Co) phase is the predominant phase in all samples. The use of the PCA favors its nanocrystallinity; however, it slows Co diffusion into the Fe matrix. Thermal analysis detects an endothermic process between 525 and 575 °C in the samples milled with C6H12 only. This is associated with the transition of the residual Fe3Co superlattice, to the stable α-Fe(Co). The effect of the residual Fe3Co at room temperature on the magnetic properties is twofold, by decreasing the saturation magnetization of Fe65Co35 but increasing both remanent magnetization and coercivity