Asymmetric Preparation of α-Quaternary Fluorinated β-keto Esters. Review

In this review, recent advances over the past decade in the preparation of fluorinated stereogenic quaternary centers on β-keto esters compounds are analyzed. Since the incorporation of fluorine and fluorinated groups is of special interest in pharmaceutical chemistry, a range of metal-catalyzed and or...

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Detalles Bibliográficos
Autores: Granados, Albert|||0000-0002-5362-5966, Vallribera, Adelina|||0000-0002-6452-4589
Tipo de recurso: artículo
Fecha de publicación:2020
País:España
Institución:Universitat Autònoma de Barcelona
Repositorio:Dipòsit Digital de Documents de la UAB
Idioma:inglés
OAI Identifier:oai:ddd.uab.cat:233192
Acceso en línea:https://ddd.uab.cat/record/233192
https://dx.doi.org/urn:doi:10.3390/molecules25143264
Access Level:acceso abierto
Palabra clave:Fluorination
Trifluoromethylation
Trifluoromethylthiolation
β-keto esters
Asymmetric
Descripción
Sumario:In this review, recent advances over the past decade in the preparation of fluorinated stereogenic quaternary centers on β-keto esters compounds are analyzed. Since the incorporation of fluorine and fluorinated groups is of special interest in pharmaceutical chemistry, a range of metal-catalyzed and organocatalyzed methods have been developed. Herein, we review the enantioselective fluorination, trifluoromethylation and trifluoromethylthiolation of 3-oxo esters. The scope, the induction of enantioselectivity and mechanistic investigations are presented.