Large area continuous multilayer graphene membrane for water desalination

[EN] This manuscript reports the preparation of a large area (84 cm2) desalination membrane based on multilayers (11 nm thickness) of B,N-codoped defective graphene. The process consists of coating a porous ceramic ?-Al2O3 support (100 nm pore size) with a continuous nanometric (50 nm) chitosan film...

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Detalles Bibliográficos
Autores: Presumido, Pedro H., Vilar, Vítor J. P., Primo Arnau, Ana Maria|||0000-0001-9205-2278, García Gómez, Hermenegildo|||0000-0002-9664-493X
Tipo de recurso: artículo
Fecha de publicación:2021
País:España
Institución:Universitat Politècnica de València (UPV)
Repositorio:RiuNet. Repositorio Institucional de la Universitat Politécnica de Valéncia
Idioma:inglés
OAI Identifier:oai:riunet.upv.es:10251/183155
Acceso en línea:https://riunet.upv.es/handle/10251/183155
Access Level:acceso abierto
Palabra clave:Desalination membrane
Multilayer graphene membrane
Subnanometric pores on graphene
Atom vacancies on graphene
Dopant removal on graphene
QUIMICA ORGANICA
Descripción
Sumario:[EN] This manuscript reports the preparation of a large area (84 cm2) desalination membrane based on multilayers (11 nm thickness) of B,N-codoped defective graphene. The process consists of coating a porous ceramic ?-Al2O3 support (100 nm pore size) with a continuous nanometric (50 nm) chitosan film containing adsorbed (NH4)3BO3. Subsequent pyrolysis in the presence of hydrogen converts chitosan into multilayer defective B,N-codoped graphene. The partial removal of B and N dopant atoms by H2 during the pyrolysis causes the generation of subnanometric pores due to atom vacancy, as determined by control experiments in the absence of this gas. A NaCl and KCl removal efficiency from brackish water higher than 95% for a permeate flux of 24.3 L m- 2 h-1 at 10 bars were achieved.