Effect of CdSe nanoparticle addition on nanostructuring of PS-b-P4VP copolymer via solvent vapour exposure

The surface morphology of poly(styrene-b-4 vinyl pyridine) (PS-b-P4VP) diblock copolymer thin films after solvent vapor annealing has been studied. Morphological features can be switched upon exposure to vapors of a solvent selective for one of the blocks. Self-assembled nanostructures such as hexag...

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Bibliographic Details
Authors: Etxeberria Altuna, Haritz, Fernández Salvador, Raquel, Zalakain, Iñaki, Mondragón Egaña, Iñaki Bixintxo, Eceiza Mendiguren, María Azanzazu, Kortaberria Altzerreka, Galder
Format: article
Publication Date:2013
Country:España
Institution:Universidad del País Vasco
Repository:Addi. Archivo Digital para la Docencia y la Investigación
OAI Identifier:oai:addi.ehu.eus:10810/65987
Online Access:http://hdl.handle.net/10810/65987
Access Level:Open access
Keyword:CdSe nanoparticles
PS-P4VP
solvent annealing
Description
Summary:The surface morphology of poly(styrene-b-4 vinyl pyridine) (PS-b-P4VP) diblock copolymer thin films after solvent vapor annealing has been studied. Morphological features can be switched upon exposure to vapors of a solvent selective for one of the blocks. Self-assembled nanostructures such as hexagonal or striped morphologies were obtained varying vapor exposure time. In addition, the effect of the presence of CdSe nanoparticles located in the P4VP block on obtained nanostructures was analyzed. Atomic force microscopy (AFM) was used for morphological characterization of the block copolymer and the nanocomposites. AFM images showed that nanostructuring was different depending on the amount of CdSe nanoparticles, due to the decrease in P4VP chain mobility.