Enabling water-based processing of graphene/alumina composites using an infiltration approach with amphiphilic triblock copolymers

Enabling the direct infiltration of freeze-cast graphene structures with water-based ceramic suspensions, otherwise prevented by graphene's intrinsic hydrophobic behaviour, can lead to the production of hierarchical graphene/ceramic composites in a cost-effective and replicable manner. In this...

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Detalles Bibliográficos
Autores: Menendez, Guillermo, Kynaston, Thomas, Villar-Garcia, Ignacio J., Gao, Min, Evans, Sam L., Rocha, Victoria G.
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2022
País:España
Institución:Consejo Superior de Investigaciones Científicas (CSIC)
Repositorio:DIGITAL.CSIC. Repositorio Institucional del CSIC
OAI Identifier:oai:digital.csic.es:10261/304635
Acceso en línea:http://hdl.handle.net/10261/304635
https://api.elsevier.com/content/abstract/scopus_id/85134754431
Access Level:acceso abierto
Palabra clave:Ceramic-based composites
Freeze-casting
Graphene oxide
Materials processing
Spark plasma sintering
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Descripción
Sumario:Enabling the direct infiltration of freeze-cast graphene structures with water-based ceramic suspensions, otherwise prevented by graphene's intrinsic hydrophobic behaviour, can lead to the production of hierarchical graphene/ceramic composites in a cost-effective and replicable manner. In this study, the addition of a triblock copolymer (PF127) in the formulation of water-based alumina slurries was used to allow the integration with reduced graphene oxide (rGO) scaffolds combining freeze-casting, wet chemistry processing and Spark Plasma Sintering. Wettability and infiltration tests were performed to optimise the composition of the ceramic suspension, leading to the preservation of alignment in embedded rGO scaffolds and maintaining channel widths of 5–15▒μm upon sintering at 1500∘ C.