Tributyl citrate as an effective plasticizer for biodegradable polymers: effect of plasticizer on free volume and transport and mechanical properties

The effectiveness of tributyl citrate (TbC) as a plasticizer for polylactide and polyhydroxybutyrate was analysed in order to improve the ductility of these polymers and make them good candidates for food packaging applications. Although the thermal and mechanical properties have been widely studied...

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Detalles Bibliográficos
Autores: Río Esteban, Francisco Javier Del, Chaos, Ana, Sangroniz, Ainara, González, Alba, Iriarte, Mariam, Sarasua, José Ramón, Etxeberria, Agustín
Tipo de recurso: artículo
Fecha de publicación:2019
País:España
Institución:Universidad Complutense de Madrid (UCM)
Repositorio:Docta Complutense
Idioma:inglés
OAI Identifier:oai:docta.ucm.es:20.500.14352/13019
Acceso en línea:https://hdl.handle.net/20.500.14352/13019
Access Level:acceso abierto
Palabra clave:538.9
Oxygen barrier properties
Poly(lactic acid)
Molecular-weight
Carbon-dioxide
Water-vapor
Poly(3-hydroxybutyrate)
Sorption
Poly(l-lactide)
Permeability
Temperature
Biodegradable polymer
Plasticizer
Free volume
Transport properties
Packaging
Física de materiales
Física del estado sólido
2211 Física del Estado Sólido
Descripción
Sumario:The effectiveness of tributyl citrate (TbC) as a plasticizer for polylactide and polyhydroxybutyrate was analysed in order to improve the ductility of these polymers and make them good candidates for food packaging applications. Although the thermal and mechanical properties have been widely studied in the literature, the effect of the plasticizer on free volume and transport properties has not been deeply analysed. The free volume was characterized using positron annihilation lifetime spectroscopy observing its linear increase with TbC content. The permeability to water vapour, oxygen and carbon dioxide was determined and the obtained results were related to the changes in glass transition temperature, level of crystallinity of the samples and free volume. This work would allow a better understanding of the effect of the plasticizer on the barrier and mechanical properties of polymers allowing the development of competitive materials for packaging applications. (c) 2018 Society of Chemical Industry