Microstructural Evolution Characterization of Fe-Nb-B Ternary Systems Processed by Ball Milling
Fe-Nb-B alloys prepared by ball milling can undergo a complex microstructural evolution during milling. In order to overcome the limitations imposed by traditional X-ray bulk analysis, a comprehensive multi-technique approach was devised to systematically characterize samples with the required resol...
| Autores: | , , , |
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| Tipo de recurso: | artículo |
| Estado: | Versión aceptada para publicación |
| Fecha de publicación: | 2009 |
| País: | España |
| Institución: | Universidad de Sevilla (US) |
| Repositorio: | idUS. Depósito de Investigación de la Universidad de Sevilla |
| OAI Identifier: | oai:idus.us.es:11441/147087 |
| Acceso en línea: | https://hdl.handle.net/11441/147087 https://doi.org/10.1080/14786430902984566 |
| Access Level: | acceso abierto |
| Palabra clave: | Amorphous alloy Ball milling FIB Nanocrystalline alloy TEM |
| Sumario: | Fe-Nb-B alloys prepared by ball milling can undergo a complex microstructural evolution during milling. In order to overcome the limitations imposed by traditional X-ray bulk analysis, a comprehensive multi-technique approach was devised to systematically characterize samples with the required resolution. A combination of in situ FIB (focused ion beam) lift-out and high-resolution ATEM (analytical transmission electron microscopy) has allowed the characterization of the phase evolution during milling. In particular, boron inclusions, not detected by X-ray diffraction, have been found to remain undissolved in the Fe matrix. |
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