Image Segmentation and 3D reconstruction for improved prediction of the sublimation rate during freeze drying

[EN] In a freeze drying process, the freezing step determines the pore size distribution within the product, which, in turn, affects the sublimation rate. Traditionally, pore analysis is carried out on SEM images by means of a manual, time-consuming approach. Here, an image segmentation technique wa...

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Bibliographic Details
Authors: Capozzi, Luigi, Arsiccio, Andrea, Sparavigna, Amelia, Pisano, Roberto, Barresi, Antonello
Format: book part
Publication Date:2018
Country:España
Institution:Universitat Politècnica de València (UPV)
Repository:RiuNet. Repositorio Institucional de la Universitat Politécnica de Valéncia
Language:English
OAI Identifier:oai:riunet.upv.es:10251/117655
Online Access:https://riunet.upv.es/handle/10251/117655
Access Level:Open access
Keyword:Drying
Dehydration
Dewatering
Emerging technologies
Products quality
Process control
Environmental
Evaporation
Sublimation
Diffusion
Energy
Intensification
Freezing
Freeze-drying
Image segmentation
3D reconstruction
Description
Summary:[EN] In a freeze drying process, the freezing step determines the pore size distribution within the product, which, in turn, affects the sublimation rate. Traditionally, pore analysis is carried out on SEM images by means of a manual, time-consuming approach. Here, an image segmentation technique was used to automatize this process and improve its reliability. A 3D structure of the cake was then reconstructed from the distribution of the super-pixels. We show that the approach herein proposed can remarkably improve prediction of the sublimation rate with respect to traditional methods.