Image Segmentation and 3D reconstruction for improved prediction of the sublimation rate during freeze drying

[EN] In a freeze drying process, the freezing step determines the pore size distribution within the product, which, in turn, affects the sublimation rate. Traditionally, pore analysis is carried out on SEM images by means of a manual, time-consuming approach. Here, an image segmentation technique wa...

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Detalhes bibliográficos
Autores: Capozzi, Luigi, Arsiccio, Andrea, Sparavigna, Amelia, Pisano, Roberto, Barresi, Antonello
Formato: capítulo de livro
Fecha de publicación:2018
País:España
Recursos:Universitat Politècnica de València (UPV)
Repositorio:RiuNet. Repositorio Institucional de la Universitat Politécnica de Valéncia
Idioma:inglés
OAI Identifier:oai:riunet.upv.es:10251/117655
Acesso em linha:https://riunet.upv.es/handle/10251/117655
Access Level:acceso abierto
Palavra-chave:Drying
Dehydration
Dewatering
Emerging technologies
Products quality
Process control
Environmental
Evaporation
Sublimation
Diffusion
Energy
Intensification
Freezing
Freeze-drying
Image segmentation
3D reconstruction
Descrição
Resumo:[EN] In a freeze drying process, the freezing step determines the pore size distribution within the product, which, in turn, affects the sublimation rate. Traditionally, pore analysis is carried out on SEM images by means of a manual, time-consuming approach. Here, an image segmentation technique was used to automatize this process and improve its reliability. A 3D structure of the cake was then reconstructed from the distribution of the super-pixels. We show that the approach herein proposed can remarkably improve prediction of the sublimation rate with respect to traditional methods.