A novel Multi‐Phase Flash Sintering (MPFS) technique for 3D complex‐shaped ceramics

This work demonstrates the first proof-of-concept of Multi-Phase Flash Sintering (MPFS). This novel tech- nique essentially consists of applying a rotating electric field to the sample by means of a multi-phase voltage source as furnace temperature increases. Several ceramic materials with different...

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Detalles Bibliográficos
Autores: Molina-Molina, Sandra, Gil González, Eva, Durán Olivencia, Francisco José, Valverde Millán, José Manuel, Perejón Pazo, Antonio, Sánchez Jiménez, Pedro Enrique, Pérez Maqueda, Luis Allan
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2022
País:España
Institución:Universidad de Sevilla (US)
Repositorio:idUS. Depósito de Investigación de la Universidad de Sevilla
OAI Identifier:oai:idus.us.es:11441/141351
Acceso en línea:https://hdl.handle.net/11441/141351
https://doi.org/10.1016/j.apmt.2021.101274
Access Level:acceso abierto
Palabra clave:Flash sintering
Alternating current
Field-assisted sintering techniques
Complex shape
Ceramic materials
Yttria-stabilized zirconia
Descripción
Sumario:This work demonstrates the first proof-of-concept of Multi-Phase Flash Sintering (MPFS). This novel tech- nique essentially consists of applying a rotating electric field to the sample by means of a multi-phase voltage source as furnace temperature increases. Several ceramic materials with different types of elec- trical conductivities are sintered within seconds at furnace temperatures much lower than those used for traditional DC flash sintering due to the higher power densities administered by a multi-phase power supply. Thus, ceramic materials are flashed at relatively lower applied voltages which minimizes un- desired phenomena such as localization and preferential current pathways. Furthermore, MPFS allows diverse electrode configurations to promote a more uniform electric field distribution, enhancing the sin- tering of 3D complex-shaped specimens. MPFS could be a true breakthrough in materials processing, as 3D complex-shaped specimens are homogeneously sintered at reduced temperatures, while keeping all the advantages of conventional flash sintering.