A novel Multi‐Phase Flash Sintering (MPFS) technique for 3D complex‐shaped ceramics

This work demonstrates the first proof-of-concept of Multi-Phase Flash Sintering (MPFS). This novel tech nique essentially consists of applying a rotating electric field to the sample by means of a multi-phase voltage source as furnace temperature increases. Several ceramic materials with different...

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Detalles Bibliográficos
Autores: Molina-Molina, Sandra, Gil González, Eva, Durán-Olivencia, F. J.*, Valverde, José Manuel, Perejón, Antonio, Sánchez-Jiménez, Pedro Enrique, Pérez-Maqueda, Luis
Tipo de recurso: artículo
Fecha de publicación:2021
País:España
Institución:Universidad Loyola Andalucía
Repositorio:Brújula
OAI Identifier:oai:repositorio.uloyola.es:20.500.12412/5460
Acceso en línea:https://hdl.handle.net/20.500.12412/5460
Access Level:acceso abierto
Palabra clave:Flash sintering
Alternating current
Field-assisted sintering techniques
Complex shape
Ceramic materials
Yttria-stabilized zirconia
Descripción
Sumario:This work demonstrates the first proof-of-concept of Multi-Phase Flash Sintering (MPFS). This novel tech nique essentially consists of applying a rotating electric field to the sample by means of a multi-phase voltage source as furnace temperature increases. Several ceramic materials with different types of elec trical conductivities are sintered within seconds at furnace temperatures much lower than those used for traditional DC flash sintering due to the higher power densities administered by a multi-phase power supply. Thus, ceramic materials are flashed at relatively lower applied voltages which minimizes un desired phenomena such as localization and preferential current pathways. Furthermore, MPFS allows diverse electrode configurations to promote a more uniform electric field distribution, enhancing the sin tering of 3D complex-shaped specimens. MPFS could be a true breakthrough in materials processing, as 3D complex-shaped specimens are homogeneously sintered at reduced temperatures, while keeping all the advantages of conventional flash sintering.