In cellulo bioorthogonal catalysis by encapsulated AuPd nanoalloys: Overcoming intracellular deactivation

Bioorthogonal metallocatalysis has opened up a xenobiotic route to perform nonenzymatic catalytic transformations in living settings. Despite their promising features, most metals are deactivated inside cells by a myriad of reactive biomolecules, including biogenic thiols, thereby limiting the catal...

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Detalles Bibliográficos
Autores: Rubio‐Ruiz, Belén, Pérez‐López, Ana M., Usón, Laura, Ortega-Liébana, M. Carmen, Valero, Teresa, Arruebo, Manuel, Hueso, José L., Sebastián, Víctor, Santamaría, Jesús, Unciti-Broceta, Asier
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2023
País:España
Institución:Consejo Superior de Investigaciones Científicas (CSIC)
Repositorio:DIGITAL.CSIC. Repositorio Institucional del CSIC
OAI Identifier:oai:digital.csic.es:10261/329906
Acceso en línea:http://hdl.handle.net/10261/329906
Access Level:acceso abierto
Palabra clave:Palladium
Gold
Nanoalloys
Catalysis
Bioorthogonal
Nanoencapsulation
Descripción
Sumario:Bioorthogonal metallocatalysis has opened up a xenobiotic route to perform nonenzymatic catalytic transformations in living settings. Despite their promising features, most metals are deactivated inside cells by a myriad of reactive biomolecules, including biogenic thiols, thereby limiting the catalytic functioning of these abiotic reagents. Here we report the development of cytocompatible alloyed AuPd nanoparticles with the capacity to elicit bioorthogonal depropargylations with high efficiency in biological media. We also show that the intracellular catalytic performance of these nanoalloys is significantly enhanced by protecting them following two different encapsulation methods. Encapsulation in mesoporous silica nanorods resulted in augmented catalyst reactivity, whereas the use of a biodegradable PLGA matrix increased nanoalloy delivery across the cell membrane. The functional potential of encapsulated AuPd was demonstrated by releasing the potent chemotherapy drug paclitaxel inside cancer cells. Nanoalloy encapsulation provides a novel methodology to develop nanoreactors capable of mediating new-to-life reactions in cells.