Development of an electrochemical sensor for coeliac disease serological markers

Coeliac disease (CD), a gluten-sensitive enteropathy, is an autoimmune disorder of the upper small intestine triggered from the gluten ingestion (cereal protein found in wheat, rye and barley) and affects 1% of the population around the globe. The ingestion of gluten, triggers the production of a se...

Descripción completa

Detalles Bibliográficos
Autor: Rosales Rivera, Luis Carlos
Tipo de recurso: tesis doctoral
Estado:Versión publicada
Fecha de publicación:2012
País:España
Institución:Universitat Rovira i virgili (URV)
Repositorio:Repositori Institucional de la Universitat Rovira i Virgili
OAI Identifier:oai:urv.cat:TDX:1138
Acceso en línea:https://hdl.handle.net/20.500.11797/TDX1138
http://hdl.handle.net/10803/96661
Access Level:acceso abierto
Palabra clave:62 - Enginyeria. Tecnologia
577 - Bioquímica. Biologia molecular. Biofísica
543 - Química analítica
Descripción
Sumario:Coeliac disease (CD), a gluten-sensitive enteropathy, is an autoimmune disorder of the upper small intestine triggered from the gluten ingestion (cereal protein found in wheat, rye and barley) and affects 1% of the population around the globe. The ingestion of gluten, triggers the production of a series of autoantibodies against gliadin (AGA) and tissue transglutaminase (anti-tTG) which can provoke inflammation and damage some parts of the intestine. The detection of those antibodies through serological testing represent a non-invasive, fast and reliable approach. The main objective of this Thesis is the development of a sensitive, rapid and cost-efficient real-sample-oriented immunosensor using thiol-self assembled monolayers on gold surfaces. Two strategies for the antigen immobilisation have been investigated: i) The use of monolayers of a carboxylic acid-ended bipodal alkanethiol, ii) The introduction of disulfide groups through three different moieties of the antigens: amine, carboxylic and hydroxyl. Both immunosensor approaches were optimized and used for the amperometric detection of CD serological markers from human serum samples.