Raw data regarding rheological characterization, pore size determination and printability of the materials employed in the study: “Genipin-Crosslinked Pectin Hydrogels: A Dual Strategy for Enhanced 3D Printability and Stability”

[Description of methods used for collection/generation of data] Rheological data. The rheological properties of all the materials were determined using a rotational rheometer (AR-G2, TA Instruments, USA) equipped with a 20 mm cross-hatched stainless steel Peltier plate geometry. Oscillatory frequenc...

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Autores: Mercado-Rico, Jorge, Pérez-Pérez, Luis, Hernández, Rebeca
Tipo de recurso: conjunto de datos
Fecha de publicación:2025
País:España
Institución:Consejo Superior de Investigaciones Científicas (CSIC)
Repositorio:DIGITAL.CSIC. Repositorio Institucional del CSIC
OAI Identifier:oai:digital.csic.es:10261/401946
Acceso en línea:http://hdl.handle.net/10261/401946
https://doi.org/10.20350/digitalCSIC/17629
Access Level:acceso abierto
Palabra clave:Frequency test
Pectin hydrogels
Printability
Pore size
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network_acronym_str ES
network_name_str España
repository_id_str
dc.title.none.fl_str_mv Raw data regarding rheological characterization, pore size determination and printability of the materials employed in the study: “Genipin-Crosslinked Pectin Hydrogels: A Dual Strategy for Enhanced 3D Printability and Stability”
title Raw data regarding rheological characterization, pore size determination and printability of the materials employed in the study: “Genipin-Crosslinked Pectin Hydrogels: A Dual Strategy for Enhanced 3D Printability and Stability”
spellingShingle Raw data regarding rheological characterization, pore size determination and printability of the materials employed in the study: “Genipin-Crosslinked Pectin Hydrogels: A Dual Strategy for Enhanced 3D Printability and Stability”
Mercado-Rico, Jorge
Frequency test
Pectin hydrogels
Printability
Pore size
Pectin hydrogels
title_short Raw data regarding rheological characterization, pore size determination and printability of the materials employed in the study: “Genipin-Crosslinked Pectin Hydrogels: A Dual Strategy for Enhanced 3D Printability and Stability”
title_full Raw data regarding rheological characterization, pore size determination and printability of the materials employed in the study: “Genipin-Crosslinked Pectin Hydrogels: A Dual Strategy for Enhanced 3D Printability and Stability”
title_fullStr Raw data regarding rheological characterization, pore size determination and printability of the materials employed in the study: “Genipin-Crosslinked Pectin Hydrogels: A Dual Strategy for Enhanced 3D Printability and Stability”
title_full_unstemmed Raw data regarding rheological characterization, pore size determination and printability of the materials employed in the study: “Genipin-Crosslinked Pectin Hydrogels: A Dual Strategy for Enhanced 3D Printability and Stability”
title_sort Raw data regarding rheological characterization, pore size determination and printability of the materials employed in the study: “Genipin-Crosslinked Pectin Hydrogels: A Dual Strategy for Enhanced 3D Printability and Stability”
dc.creator.none.fl_str_mv Mercado-Rico, Jorge
Pérez-Pérez, Luis
Hernández, Rebeca
author Mercado-Rico, Jorge
author_facet Mercado-Rico, Jorge
Pérez-Pérez, Luis
Hernández, Rebeca
author_role author
author2 Pérez-Pérez, Luis
Hernández, Rebeca
author2_role author
author
dc.contributor.none.fl_str_mv Ministerio de Ciencia, Innovación y Universidades (España)
Comunidad de Madrid
Mercado-Rico, Jorge
Pérez-Pérez, Luis
Hernández, Rebeca [0000-0001-7332-0134]
rhernandez@ictp.csic.es
Consejo Superior de Investigaciones Científicas [https://ror.org/02gfc7t72]
dc.subject.none.fl_str_mv Frequency test
Pectin hydrogels
Printability
Pore size
Pectin hydrogels
topic Frequency test
Pectin hydrogels
Printability
Pore size
Pectin hydrogels
description [Description of methods used for collection/generation of data] Rheological data. The rheological properties of all the materials were determined using a rotational rheometer (AR-G2, TA Instruments, USA) equipped with a 20 mm cross-hatched stainless steel Peltier plate geometry. Oscillatory frequency sweep tests were conducted on pectin-genipin hydrogels swollen at equilibrium over a frequency range of 0.01–10 Hz, at a temperature of 25 ºC and at a constant strain of 1%, located within the linear viscoelastic region (LVR). An oscillatory amplitude sweep (1 Hz; γ = 0.01%–500%) was performed to determine the critical strain, defined as the point at which a 5% decrease in the storage modulus (G′) is observed. Subsequently, frequency sweep tests (1% strain, 0.01–100 Hz) were carried out to measure the storage modulus (G′) and loss modulus (G″). Finally, hydrogel recovery test varying the strain from 1% to 200% at a constant frequency of 1 Hz, applying 2 cycles at high strain. Printability tests. Scaffolds were fabricated via 3D printing using a Creality Ender 3 Pro filament printer, which was adapted to enable the extrusion of polymeric hydrogels. The uniformity factor (U) was used to evaluate how uniform the filament was compared to a perfectly straight filament. Digimizer software was used to manually measure the outer edge on both sides of the filament. This length was then divided by the length of the reference line to calculate the uniformity factor (equation 2), which indicates whether the filament is uniform (U = 1) or non-uniform (U > 1). U"\=" (length"\ "of"\ "printed"\ "filament"\ ")/(length"\ "of"\ "theorical"\ "straight"\ "filament) (Equation 1) For the determination of the printability index, Pr, a single layer cylindrical scaffold was printed with an internal design configured to form 12 squares with a side length of 3 mm each. The area of each internal square was quantified using Digimizer software, and these values were used to calculate the average printability index (Pr) according to equation 3. Based on this index, three gelation states are identified: insufficient gelation (Pr < 1), adequate gelation (Pr = 1), and excessive gelation (Pr > 1). Pr"\=" π/4 x 1/C "\=" L^2/16A "\ "(Equation"\ " 2) Pore size. Pore size was quantified using ImageJ. Micrographs were calibrated with the scale bar, and image preprocessing (contrast enhancement and threshold adjustment) was applied to delineate pore boundaries. Approximately 45 pores were analyzed per sample, and the equivalent circular diameter was calculated from the pore area. Results were reported as mean ± standard deviation (SD) to describe pore size distribution.
publishDate 2025
dc.date.none.fl_str_mv 2025
2025
2025
dc.type.none.fl_str_mv info:eu-repo/semantics/dataset
http://purl.org/coar/resource_type/c_ddb1
format dataset
dc.identifier.none.fl_str_mv http://hdl.handle.net/10261/401946
https://doi.org/10.20350/digitalCSIC/17629
url http://hdl.handle.net/10261/401946
https://doi.org/10.20350/digitalCSIC/17629
dc.language.none.fl_str_mv Inglés
language_invalid_str_mv Inglés
dc.relation.none.fl_str_mv #PLACEHOLDER_PARENT_METADATA_VALUE#
#PLACEHOLDER_PARENT_METADATA_VALUE#
#PLACEHOLDER_PARENT_METADATA_VALUE#
info:eu-repo/grantAgreement/AEI/Plan Estatal de Investigación Científica y Técnica y de Innovación 2017-2020/PID2020-113045GB-C22
info:eu-repo/grantAgreement/AEI/Plan Estatal de Investigación Científica y Técnica y de Innovación 2021-2023/PID2023-149734NB-C21
TEC-2024/TEC-102/CM
Sí
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv Excel, Origin or any other program capable of open files -.txt, -.csv and -.dat.
Only CSV, TXT and DAT files
dc.publisher.none.fl_str_mv DIGITAL.CSIC
publisher.none.fl_str_mv DIGITAL.CSIC
dc.source.none.fl_str_mv reponame:DIGITAL.CSIC. Repositorio Institucional del CSIC
instname:Consejo Superior de Investigaciones Científicas (CSIC)
instname_str Consejo Superior de Investigaciones Científicas (CSIC)
reponame_str DIGITAL.CSIC. Repositorio Institucional del CSIC
collection DIGITAL.CSIC. Repositorio Institucional del CSIC
repository.name.fl_str_mv
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spelling Raw data regarding rheological characterization, pore size determination and printability of the materials employed in the study: “Genipin-Crosslinked Pectin Hydrogels: A Dual Strategy for Enhanced 3D Printability and Stability”Mercado-Rico, JorgePérez-Pérez, LuisHernández, RebecaFrequency testPectin hydrogelsPrintabilityPore sizePectin hydrogels[Description of methods used for collection/generation of data] Rheological data. The rheological properties of all the materials were determined using a rotational rheometer (AR-G2, TA Instruments, USA) equipped with a 20 mm cross-hatched stainless steel Peltier plate geometry. Oscillatory frequency sweep tests were conducted on pectin-genipin hydrogels swollen at equilibrium over a frequency range of 0.01–10 Hz, at a temperature of 25 ºC and at a constant strain of 1%, located within the linear viscoelastic region (LVR). An oscillatory amplitude sweep (1 Hz; γ = 0.01%–500%) was performed to determine the critical strain, defined as the point at which a 5% decrease in the storage modulus (G′) is observed. Subsequently, frequency sweep tests (1% strain, 0.01–100 Hz) were carried out to measure the storage modulus (G′) and loss modulus (G″). Finally, hydrogel recovery test varying the strain from 1% to 200% at a constant frequency of 1 Hz, applying 2 cycles at high strain. Printability tests. Scaffolds were fabricated via 3D printing using a Creality Ender 3 Pro filament printer, which was adapted to enable the extrusion of polymeric hydrogels. The uniformity factor (U) was used to evaluate how uniform the filament was compared to a perfectly straight filament. Digimizer software was used to manually measure the outer edge on both sides of the filament. This length was then divided by the length of the reference line to calculate the uniformity factor (equation 2), which indicates whether the filament is uniform (U = 1) or non-uniform (U > 1). U"\=" (length"\ "of"\ "printed"\ "filament"\ ")/(length"\ "of"\ "theorical"\ "straight"\ "filament) (Equation 1) For the determination of the printability index, Pr, a single layer cylindrical scaffold was printed with an internal design configured to form 12 squares with a side length of 3 mm each. The area of each internal square was quantified using Digimizer software, and these values were used to calculate the average printability index (Pr) according to equation 3. Based on this index, three gelation states are identified: insufficient gelation (Pr < 1), adequate gelation (Pr = 1), and excessive gelation (Pr > 1). Pr"\=" π/4 x 1/C "\=" L^2/16A "\ "(Equation"\ " 2) Pore size. Pore size was quantified using ImageJ. Micrographs were calibrated with the scale bar, and image preprocessing (contrast enhancement and threshold adjustment) was applied to delineate pore boundaries. Approximately 45 pores were analyzed per sample, and the equivalent circular diameter was calculated from the pore area. Results were reported as mean ± standard deviation (SD) to describe pore size distribution.[Methods for processing the data] The files contain raw data obtained through rheological measurements, pore size determination and printability tests are organized in EXCEL files to improve visualization.This dataset contains raw data from obtained through oscillatory rheological measurements, pore size determination and printability tests organized in EXCEL files and employed in the study “Genipin-Crosslinked Pectin Hydrogels: A Dual Strategy for Enhanced 3D Printability and Stability”This research has been funded by the projects PID2020-113045GB-C22 and PID2023-149734NB-C21 by MCIN/AEI/10.13039/501100011033, the “Industrial Doctorate” call (DIN2019-010868), and the DIGIMATER-CM project (TEC-2024/TEC-102) funded by the Community of MadridPeer reviewedDIGITAL.CSICMinisterio de Ciencia, Innovación y Universidades (España)Comunidad de MadridMercado-Rico, JorgePérez-Pérez, LuisHernández, Rebeca [0000-0001-7332-0134]rhernandez@ictp.csic.esConsejo Superior de Investigaciones Científicas [https://ror.org/02gfc7t72]202520252025info:eu-repo/semantics/datasethttp://purl.org/coar/resource_type/c_ddb1Excel, Origin or any other program capable of open files -.txt, -.csv and -.dat.Only CSV, TXT and DAT fileshttp://hdl.handle.net/10261/401946https://doi.org/10.20350/digitalCSIC/17629reponame:DIGITAL.CSIC. Repositorio Institucional del CSICinstname:Consejo Superior de Investigaciones Científicas (CSIC)Inglés#PLACEHOLDER_PARENT_METADATA_VALUE##PLACEHOLDER_PARENT_METADATA_VALUE##PLACEHOLDER_PARENT_METADATA_VALUE#info:eu-repo/grantAgreement/AEI/Plan Estatal de Investigación Científica y Técnica y de Innovación 2017-2020/PID2020-113045GB-C22info:eu-repo/grantAgreement/AEI/Plan Estatal de Investigación Científica y Técnica y de Innovación 2021-2023/PID2023-149734NB-C21TEC-2024/TEC-102/CMSíinfo:eu-repo/semantics/openAccessoai:digital.csic.es:10261/4019462026-05-22T06:33:51Z
score 15.812429

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