Electrochemical fingerprint of archeological lead silicate glasses using the voltammetry of microparticles approach

9 págs.; 14 figs.; 1 tab.

Detalles Bibliográficos
Autores: Doménech-Carbó, A., Villegas Broncano, María Ángeles, Agua Martínez, Fernando, Martínez-Ramírez, S., Doménech-Carbó, M.T., Martínez, B., Lloyd, I.
Tipo de recurso: artículo
Estado:Versión aceptada para publicación
Fecha de publicación:2016
País:España
Institución:Consejo Superior de Investigaciones Científicas (CSIC)
Repositorio:DIGITAL.CSIC. Repositorio Institucional del CSIC
OAI Identifier:oai:digital.csic.es:10261/151215
Acceso en línea:http://hdl.handle.net/10261/151215
Access Level:acceso abierto
Palabra clave:Provenance
Archeology
Voltammetry of microparti-cles
Lead glass
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spelling Electrochemical fingerprint of archeological lead silicate glasses using the voltammetry of microparticles approachDoménech-Carbó, A.Villegas Broncano, María ÁngelesAgua Martínez, FernandoMartínez-Ramírez, S.Doménech-Carbó, M.T.Martínez, B.Lloyd, I.ProvenanceArcheologyVoltammetry of microparti-clesLead glass9 págs.; 14 figs.; 1 tab.The application of a solid-state electrochemical technique, voltammetry of microparticles (VMP), for studying archeological lead glass is described. Upon attachment to graphite electrodes immersed into aqueous acetate buffer, characteristic voltammetric profiles were obtained for submicrosamples of archeological glasses dated between the 9th and 19th centuries. Bivariate and multivariate chemometric analyses of the VMP data allowed us to characterize individual workshops/provenances which enabled a clear discrimination between soda-rich and potash-rich glasses. An analysis of the VMP data, combined by XRF, FESEM, AFM and ATR-FTIR and Micro-Raman spectroscopies, denoted the presence of Pb(IV) centers accompanying network-former and network-modifier Pb(II). © 2016 The American Ceramic SocietyFinancial support from the MINECO Projects CTQ2014-53736-C3-1-P,CTQ2014-53736-C3-2-P and MAT2015-65445-C2-2-R, which are supportedwith ERDF funds is gratefully acknowledged. Likewise financial support ofthe Comunidad de Madrid and structural funds of the EU through ProgramaGeomateriales 2 ref. S2013/MIT-2914 is acknowledged. The authors thank the Sección de Investigación Arqueológica Municipal de Valencia for kindly authorizing sampling to carry out this research. The authors also thank Dr.Jose Luis Moya Lopez and Mr. Manuel Planes Insausti (Microscopy Serviceof the Universitat Politécnica de Valencia) for their technical support.Peer ReviewedAmerican Ceramic SocietyMinisterio de Economía y Competitividad (España)Universidad Politécnica de ValenciaComunidad de MadridConsejo Superior de Investigaciones Científicas [https://ror.org/02gfc7t72]2017201720162017info:eu-repo/semantics/articlehttp://purl.org/coar/resource_type/c_6501Postprintinfo:eu-repo/semantics/acceptedVersionhttp://hdl.handle.net/10261/151215reponame:DIGITAL.CSIC. Repositorio Institucional del CSICinstname:Consejo Superior de Investigaciones Científicas (CSIC)Inglés#PLACEHOLDER_PARENT_METADATA_VALUE##PLACEHOLDER_PARENT_METADATA_VALUE##PLACEHOLDER_PARENT_METADATA_VALUE##PLACEHOLDER_PARENT_METADATA_VALUE#info:eu-repo/grantAgreement/MINECO/Plan Estatal de Investigación Científica y Técnica y de Innovación 2013-2016/CTQ2014-53736-C3-1-Pinfo:eu-repo/grantAgreement/MINECO/Plan Estatal de Investigación Científica y Técnica y de Innovación 2013-2016/CTQ2014-53736-C3-2-PS2013/MIT-2914/GEOMATERIALES 2-CMinfo:eu-repo/grantAgreement/MINECO/Plan Estatal de Investigación Científica y Técnica y de Innovación 2013-2016/MAT2015-65445-C2-2-Rhttp://doi.org/10.1111/jace.14430Síinfo:eu-repo/semantics/openAccessoai:digital.csic.es:10261/1512152026-05-22T06:33:51Z
dc.title.none.fl_str_mv Electrochemical fingerprint of archeological lead silicate glasses using the voltammetry of microparticles approach
title Electrochemical fingerprint of archeological lead silicate glasses using the voltammetry of microparticles approach
spellingShingle Electrochemical fingerprint of archeological lead silicate glasses using the voltammetry of microparticles approach
Doménech-Carbó, A.
Provenance
Archeology
Voltammetry of microparti-cles
Lead glass
title_short Electrochemical fingerprint of archeological lead silicate glasses using the voltammetry of microparticles approach
title_full Electrochemical fingerprint of archeological lead silicate glasses using the voltammetry of microparticles approach
title_fullStr Electrochemical fingerprint of archeological lead silicate glasses using the voltammetry of microparticles approach
title_full_unstemmed Electrochemical fingerprint of archeological lead silicate glasses using the voltammetry of microparticles approach
title_sort Electrochemical fingerprint of archeological lead silicate glasses using the voltammetry of microparticles approach
dc.creator.none.fl_str_mv Doménech-Carbó, A.
Villegas Broncano, María Ángeles
Agua Martínez, Fernando
Martínez-Ramírez, S.
Doménech-Carbó, M.T.
Martínez, B.
Lloyd, I.
author Doménech-Carbó, A.
author_facet Doménech-Carbó, A.
Villegas Broncano, María Ángeles
Agua Martínez, Fernando
Martínez-Ramírez, S.
Doménech-Carbó, M.T.
Martínez, B.
Lloyd, I.
author_role author
author2 Villegas Broncano, María Ángeles
Agua Martínez, Fernando
Martínez-Ramírez, S.
Doménech-Carbó, M.T.
Martínez, B.
Lloyd, I.
author2_role author
author
author
author
author
author
dc.contributor.none.fl_str_mv Ministerio de Economía y Competitividad (España)
Universidad Politécnica de Valencia
Comunidad de Madrid
Consejo Superior de Investigaciones Científicas [https://ror.org/02gfc7t72]
dc.subject.none.fl_str_mv Provenance
Archeology
Voltammetry of microparti-cles
Lead glass
topic Provenance
Archeology
Voltammetry of microparti-cles
Lead glass
description 9 págs.; 14 figs.; 1 tab.
publishDate 2016
dc.date.none.fl_str_mv 2016
2017
2017
2017
dc.type.none.fl_str_mv info:eu-repo/semantics/article
http://purl.org/coar/resource_type/c_6501
Postprint
info:eu-repo/semantics/acceptedVersion
format article
status_str acceptedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/10261/151215
url http://hdl.handle.net/10261/151215
dc.language.none.fl_str_mv Inglés
language_invalid_str_mv Inglés
dc.relation.none.fl_str_mv #PLACEHOLDER_PARENT_METADATA_VALUE#
#PLACEHOLDER_PARENT_METADATA_VALUE#
#PLACEHOLDER_PARENT_METADATA_VALUE#
#PLACEHOLDER_PARENT_METADATA_VALUE#
info:eu-repo/grantAgreement/MINECO/Plan Estatal de Investigación Científica y Técnica y de Innovación 2013-2016/CTQ2014-53736-C3-1-P
info:eu-repo/grantAgreement/MINECO/Plan Estatal de Investigación Científica y Técnica y de Innovación 2013-2016/CTQ2014-53736-C3-2-P
S2013/MIT-2914/GEOMATERIALES 2-CM
info:eu-repo/grantAgreement/MINECO/Plan Estatal de Investigación Científica y Técnica y de Innovación 2013-2016/MAT2015-65445-C2-2-R
http://doi.org/10.1111/jace.14430
Sí
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.publisher.none.fl_str_mv American Ceramic Society
publisher.none.fl_str_mv American Ceramic Society
dc.source.none.fl_str_mv reponame:DIGITAL.CSIC. Repositorio Institucional del CSIC
instname:Consejo Superior de Investigaciones Científicas (CSIC)
instname_str Consejo Superior de Investigaciones Científicas (CSIC)
reponame_str DIGITAL.CSIC. Repositorio Institucional del CSIC
collection DIGITAL.CSIC. Repositorio Institucional del CSIC
repository.name.fl_str_mv
repository.mail.fl_str_mv
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