Organometallic Ni(II), Ni(III), and Ni(IV) complexes relevant to carbon-carbon and carbon-oxygen bond formation reactions

Herein, the pyridinophanetetradentate ligand 3,6,9-trimethyl-3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1(15),11,13-triene, PyNMe3, is used to isolate and structurally characterize well-defined organometallic Ni(II) and Ni(III) complexes bearing the cycloneophyl fragment, an alkyl/aryl C-donor ligand....

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Detalles Bibliográficos
Autores: Magallón, Carla, Griego, Leonel, Hu, C. H., Company Casadevall, Anna, Ribas Salamaña, Xavi, Mirica, Liviu M.
Tipo de recurso: artículo
Estado:Versión aceptada para publicación
Fecha de publicación:2022
País:España
Institución:Varias* (Consorci de Biblioteques Universitáries de Catalunya, Centre de Serveis Científics i Acadèmics de Catalunya)
Repositorio:Recercat. Dipósit de la Recerca de Catalunya
OAI Identifier:oai:recercat.cat:10256/20852
Acceso en línea:http://hdl.handle.net/10256/20852
Access Level:acceso abierto
Palabra clave:Compostos organometàl·lics
Organometallic compounds
Descripción
Sumario:Herein, the pyridinophanetetradentate ligand 3,6,9-trimethyl-3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1(15),11,13-triene, PyNMe3, is used to isolate and structurally characterize well-defined organometallic Ni(II) and Ni(III) complexes bearing the cycloneophyl fragment, an alkyl/aryl C-donor ligand. Furthermore, spectroscopic and cryo-mass spectrometry studies suggest the formation of a transient Ni(IV) organometallic complex, and its relevance to C-C and C-O bond formation reactivity studies is discussed