Selective Synthesis of Phenanthrenes and Dihydrophenanthrenes via Gold-Catalyzed Cycloisomerization of Biphenyl Embedded Trienynes

Readily available o′-alkenyl-o-alkynylbiaryls, a particular type of 1,7-enynes, undergo a selective cycloisomerization reaction in the presence of a gold(I) catalyst to give interesting phenanthrene and dihydrophenanthrene derivatives in high yields. The solvent used provokes a switch in the evoluti...

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Detalles Bibliográficos
Autores: Milián López, Ana|||0000-0001-6101-077X, García García, Patricia|||0000-0003-3671-5828, Pérez Redondo, Adrián|||0000-0002-0086-8825, Sanz, Roberto, Vaquero López, Juan José|||0000-0002-3820-9673, Fernández Rodríguez, Manuel Ángel|||0000-0002-0120-5599
Tipo de recurso: artículo
Fecha de publicación:2020
País:España
Institución:Universidad de Alcalá (UAH)
Repositorio:e_Buah Biblioteca Digital Universidad de Alcalá
Idioma:inglés
OAI Identifier:oai:ebuah.uah.es:10017/49347
Acceso en línea:http://hdl.handle.net/10017/49347
https://dx.doi.org/10.1021/acs.orglett.0c03067
Access Level:acceso abierto
Palabra clave:Phenanthrenes
Gold
Catalysis
Cycloisomerization
Trienynes
Química
Chemistry
Descripción
Sumario:Readily available o′-alkenyl-o-alkynylbiaryls, a particular type of 1,7-enynes, undergo a selective cycloisomerization reaction in the presence of a gold(I) catalyst to give interesting phenanthrene and dihydrophenanthrene derivatives in high yields. The solvent used provokes a switch in the evolution of the gold intermediate and plays a key role in the reaction outcome.