Synthesis of Phenanthrene-based Polycycles by Gold (I)-Catalyzed Cyclization of Biphenyl Embedded Trienynes

Gold(I)-catalyzed cyclization of o-alkenyl-o?-alkynylbiaryls in the presence of external or internal nucleophiles provides a straightforward access to phenanthrene-based polycycles, which are of considerable interest in materials science. Thus, their reactions with alcohols yield functionalized dihy...

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Detalles Bibliográficos
Autores: Milián López, Ana|||0000-0001-6101-077X, García García, Patricia|||0000-0003-3671-5828, Vaquero López, Juan José|||0000-0002-3820-9673, Sanz, Roberto, Fernández Rodríguez, Manuel Ángel|||0000-0002-0120-5599
Tipo de recurso: artículo
Fecha de publicación:2022
País:España
Institución:Universidad de Alcalá (UAH)
Repositorio:e_Buah Biblioteca Digital Universidad de Alcalá
Idioma:inglés
OAI Identifier:oai:ebuah.uah.es:10017/59160
Acceso en línea:http://hdl.handle.net/10017/59160
https://dx.doi.org/10.1002/adsc.202200887
Access Level:acceso abierto
Palabra clave:Phenanthrenes
Gold
Catalysis
Cycloisomerization
Trienynes
Química
Chemistry
Descripción
Sumario:Gold(I)-catalyzed cyclization of o-alkenyl-o?-alkynylbiaryls in the presence of external or internal nucleophiles provides a straightforward access to phenanthrene-based polycycles, which are of considerable interest in materials science. Thus, their reactions with alcohols yield functionalized dihydrophenanthrenes, in a process that can also be carried out intramolecularly, to provide phenanthrene-derived heteropolycyclic compounds. Moreover, benzo[b]triphenylenes can be synthesized from o-methoxyvinyl-o?-alkynylbiaryls, in a reaction in which an (hetero)aryl substituent at the triple bond acts as an internal nucleophile.