Crystallization of M2SiO4 (M = Ni, Co) olivine solid solutions from Na2CoxNi1-xSi4O10 (0.0 ≤ x ≤ 1.0) compositions

The crystallization of olivine solid solutions from Na2CoxNi1-xSi4O10 (0.0 ≤ x ≤ 1.0) compositions, synthesized via the chemical co-precipitation method, was studied. These materials enable a gradation of the green to blue coloration in both powdered and enamelled forms. The presence of additional c...

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Detalhes bibliográficos
Autores: Tena, M. A., Abdelbaky, Mohammed S. M., Trobajo, Camino, García-Granda, Santiago
Formato: artículo
Estado:Versión publicada
Fecha de publicación:2025
País:España
Recursos:Consejo Superior de Investigaciones Científicas (CSIC)
Repositorio:DIGITAL.CSIC. Repositorio Institucional del CSIC
OAI Identifier:oai:digital.csic.es:10261/411958
Acesso em linha:http://hdl.handle.net/10261/411958
Access Level:acceso abierto
Palavra-chave:Olivine
Pigments
Solid solutions
Descrição
Resumo:The crystallization of olivine solid solutions from Na2CoxNi1-xSi4O10 (0.0 ≤ x ≤ 1.0) compositions, synthesized via the chemical co-precipitation method, was studied. These materials enable a gradation of the green to blue coloration in both powdered and enamelled forms. The presence of additional crystalline phases alongside these olivine solid solutions at 1000 and 1200 °C does not decrease the intensity of the colour. This allows a reduction in the amount of Ni(II) and Co(II) in the compositions. The crystallization of olivine begins at 800 °C in a pink phase with 0.4 ≤ x ≤ 0.8 in compositions. Its spectra can be interpreted as the effect of combining the colour contributions of Ni(II) and Co(II) ions in octahedral sites. At 1000 and 1200 °C, compositions with x > 0.2 exhibit a blue colour, and an additional spectral band attributed to Co(II) ions in tetrahedral coordination is observed.