Self-assembly and lateral cobalt coordination of a five-fold symmetric cyanostar macrocycle on a Au(111) surface

The functionalization of solid surfaces with responsive macrocyclic compounds is a key strategy for developing advanced functional materials, with applications in molecular sensing, catalysis, and nanoscale electronics. Here,we report the self-assembly and lateral cobalt coordination, on an Au(111)...

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Autores: Černá, Lenka, Martínez García, Miguel, Mathialagan, Shanmugasibi K., Parreiras, Sofía O., Lauwaet, Koen, Urgel, José Ignacio, Gallardo, Aurelio, Flood, Amar H., Torres Cebada, Tomás, Gallego, José M., Bottari, Giovanni, Écija, David
Tipo de recurso: artículo
Fecha de publicación:2025
País:España
Institución:Universidad Autónoma de Madrid
Repositorio:Biblos-e Archivo. Repositorio Institucional de la UAM
Idioma:inglés
OAI Identifier:oai:repositorio.uam.es:10486/749000
Acceso en línea:https://hdl.handle.net/10486/749000
https://dx.doi.org/10.1002/chem.202503051
Access Level:acceso abierto
Palabra clave:cyanostar
metal-ligand coordination
on-surface chemistry
scanning tunneling microscopy
self-assembly
Química
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spelling Self-assembly and lateral cobalt coordination of a five-fold symmetric cyanostar macrocycle on a Au(111) surfaceČerná, LenkaMartínez García, MiguelMathialagan, Shanmugasibi K.Parreiras, Sofía O.Lauwaet, KoenUrgel, José IgnacioGallardo, AurelioFlood, Amar H.Torres Cebada, TomásGallego, José M.Bottari, GiovanniÉcija, Davidcyanostarmetal-ligand coordinationon-surface chemistryscanning tunneling microscopyself-assemblyQuímicaThe functionalization of solid surfaces with responsive macrocyclic compounds is a key strategy for developing advanced functional materials, with applications in molecular sensing, catalysis, and nanoscale electronics. Here,we report the self-assembly and lateral cobalt coordination, on an Au(111) surface and under ultra-high vacuum conditions, of a fivefold symmetric cyanostar macrocycle, a class of anion recognition molecules. This represents the first example of a close-packed regular assembly of a pentagonal macrocycle at the solid-vacuum interfaceThis project has received funding from the Spanish Ministerio de Ciencia e Innovación (grant PID2022-136961NB-I00). T.T. and G.B. acknowledge financial support from the Spanish MCIN/AEI/10.13039/501100011033 and European Union NextGenerationEU/PRTR (TED2021-131255B-C43), MICIU/AEI/10.13039/501100011033/FEDER, UE (PID2023-151167NBI00), the Comunidad de Madrid and the Spanish State through the Recovery, Transformation and Resilience Plan [“Materiales Disruptivos Bidimensionales (2D)” (MAD2D-CM) (UAM1)-MRR Materiales Avanzados], and the European Union through the Next Generation EU funds. We also acknowledge the support from the ‘(MAD2D-CM)-IMDEA-Nanociencia’ and ‘(MAD2D-CM)-UCM’ projects funded by Comunidad de Madrid, by the Recovery, Transformation and Resilience Plan, and by NextGenerationEU from the European Union. We thank funding from PERTE Chip project PDC2023-145871-I00. A.H.F. acknowledges support from the NSF (CHE-2403941). The authors thank Comunidad de Madrid through the “Programa de Actividades de I+D” (TEC-2024/TEC-459, SYNMOLMAT-CM)WileyDepartamento de Química OrgánicaFacultad de CienciasComunidad de MadridGobierno de España20252025-12-03research articlehttp://purl.org/coar/resource_type/c_2df8fbb1VoRhttp://purl.org/coar/version/c_970fb48d4fbd8a85info:eu-repo/semantics/articleapplication/pdfhttps://hdl.handle.net/10486/749000https://dx.doi.org/10.1002/chem.202503051reponame:Biblos-e Archivo. Repositorio Institucional de la UAMinstname:Universidad Autónoma de MadridInglésengopen accesshttp://purl.org/coar/access_right/c_abf2Attribution 4.0 Internationalhttp://creativecommons.org/licenses/by/4.0/info:eu-repo/semantics/openAccessoai:repositorio.uam.es:10486/7490002026-06-23T12:46:27Z
dc.title.none.fl_str_mv Self-assembly and lateral cobalt coordination of a five-fold symmetric cyanostar macrocycle on a Au(111) surface
title Self-assembly and lateral cobalt coordination of a five-fold symmetric cyanostar macrocycle on a Au(111) surface
spellingShingle Self-assembly and lateral cobalt coordination of a five-fold symmetric cyanostar macrocycle on a Au(111) surface
Černá, Lenka
cyanostar
metal-ligand coordination
on-surface chemistry
scanning tunneling microscopy
self-assembly
Química
title_short Self-assembly and lateral cobalt coordination of a five-fold symmetric cyanostar macrocycle on a Au(111) surface
title_full Self-assembly and lateral cobalt coordination of a five-fold symmetric cyanostar macrocycle on a Au(111) surface
title_fullStr Self-assembly and lateral cobalt coordination of a five-fold symmetric cyanostar macrocycle on a Au(111) surface
title_full_unstemmed Self-assembly and lateral cobalt coordination of a five-fold symmetric cyanostar macrocycle on a Au(111) surface
title_sort Self-assembly and lateral cobalt coordination of a five-fold symmetric cyanostar macrocycle on a Au(111) surface
dc.creator.none.fl_str_mv Černá, Lenka
Martínez García, Miguel
Mathialagan, Shanmugasibi K.
Parreiras, Sofía O.
Lauwaet, Koen
Urgel, José Ignacio
Gallardo, Aurelio
Flood, Amar H.
Torres Cebada, Tomás
Gallego, José M.
Bottari, Giovanni
Écija, David
author Černá, Lenka
author_facet Černá, Lenka
Martínez García, Miguel
Mathialagan, Shanmugasibi K.
Parreiras, Sofía O.
Lauwaet, Koen
Urgel, José Ignacio
Gallardo, Aurelio
Flood, Amar H.
Torres Cebada, Tomás
Gallego, José M.
Bottari, Giovanni
Écija, David
author_role author
author2 Martínez García, Miguel
Mathialagan, Shanmugasibi K.
Parreiras, Sofía O.
Lauwaet, Koen
Urgel, José Ignacio
Gallardo, Aurelio
Flood, Amar H.
Torres Cebada, Tomás
Gallego, José M.
Bottari, Giovanni
Écija, David
author2_role author
author
author
author
author
author
author
author
author
author
author
dc.contributor.none.fl_str_mv Departamento de Química Orgánica
Facultad de Ciencias
Comunidad de Madrid
Gobierno de España
dc.subject.none.fl_str_mv cyanostar
metal-ligand coordination
on-surface chemistry
scanning tunneling microscopy
self-assembly
Química
topic cyanostar
metal-ligand coordination
on-surface chemistry
scanning tunneling microscopy
self-assembly
Química
description The functionalization of solid surfaces with responsive macrocyclic compounds is a key strategy for developing advanced functional materials, with applications in molecular sensing, catalysis, and nanoscale electronics. Here,we report the self-assembly and lateral cobalt coordination, on an Au(111) surface and under ultra-high vacuum conditions, of a fivefold symmetric cyanostar macrocycle, a class of anion recognition molecules. This represents the first example of a close-packed regular assembly of a pentagonal macrocycle at the solid-vacuum interface
publishDate 2025
dc.date.none.fl_str_mv 2025
2025-12-03
dc.type.none.fl_str_mv research article
http://purl.org/coar/resource_type/c_2df8fbb1
VoR
http://purl.org/coar/version/c_970fb48d4fbd8a85
dc.type.openaire.fl_str_mv info:eu-repo/semantics/article
format article
dc.identifier.none.fl_str_mv https://hdl.handle.net/10486/749000
https://dx.doi.org/10.1002/chem.202503051
url https://hdl.handle.net/10486/749000
https://dx.doi.org/10.1002/chem.202503051
dc.language.none.fl_str_mv Inglés
eng
language_invalid_str_mv Inglés
language eng
dc.rights.none.fl_str_mv open access
http://purl.org/coar/access_right/c_abf2
Attribution 4.0 International
http://creativecommons.org/licenses/by/4.0/
dc.rights.openaire.fl_str_mv info:eu-repo/semantics/openAccess
rights_invalid_str_mv open access
http://purl.org/coar/access_right/c_abf2
Attribution 4.0 International
http://creativecommons.org/licenses/by/4.0/
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
dc.publisher.none.fl_str_mv Wiley
publisher.none.fl_str_mv Wiley
dc.source.none.fl_str_mv reponame:Biblos-e Archivo. Repositorio Institucional de la UAM
instname:Universidad Autónoma de Madrid
instname_str Universidad Autónoma de Madrid
reponame_str Biblos-e Archivo. Repositorio Institucional de la UAM
collection Biblos-e Archivo. Repositorio Institucional de la UAM
repository.name.fl_str_mv
repository.mail.fl_str_mv
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