Ethanol gas sensing mechanisms of p-type NiO at room temperature

Conductometric gas sensors based on metal oxide semiconductors (MOS) usually require high temperature operation, increasing their energy consumption and limiting their applicability. However, room temperature operation with these devices still remains a challenge in many sensor-analyte systems due i...

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Detalles Bibliográficos
Autores: Bartolomé Vílchez, Javier, Taeño González, María, Martínez Casado, María Ruth, Maestre Varea, David, Cremades Rodríguez, Ana Isabel
Tipo de recurso: artículo
Fecha de publicación:2022
País:España
Institución:Universidad Complutense de Madrid (UCM)
Repositorio:Docta Complutense
Idioma:inglés
OAI Identifier:oai:docta.ucm.es:20.500.14352/72449
Acceso en línea:https://hdl.handle.net/20.500.14352/72449
Access Level:acceso abierto
Palabra clave:538.9
Nickel oxide
Conductometric gas sensing
Charge transfer
Adsorption
Electron backscattered diffraction
Física (Física)
Física del estado sólido
22 Física
2211 Física del Estado Sólido
Descripción
Sumario:Conductometric gas sensors based on metal oxide semiconductors (MOS) usually require high temperature operation, increasing their energy consumption and limiting their applicability. However, room temperature operation with these devices still remains a challenge in many sensor-analyte systems due in part to the low or null response and recovery speeds obtained at this temperature. In this work, the conductometric response of ptype NiO ceramic samples to ethanol is studied under room temperature operation. An anomalous response consisting in an unexpected resistance decrease upon ethanol exposure is observed depending on sample texturing, which is tuned by changing the temperature at which the samples are synthesized. This anomalous response is characterized by fast response and recovery times. A model based on two competing mechanisms, consisting in either an electron transfer from NiO to the ethanol molecule or the catalytic decomposition of adsorbed ethanol, is proposed to explain the observed anomalous response. Extending this model to other MOS could pave the way for fast sensors operating at room temperature.