Carbon-fiber tips for scanning probe microscopes and molecular electronics experiments

We fabricate and characterize carbon-fiber tips for their use in combined scanning tunneling and force microscopy based on piezoelectric quartz tuning fork force sensors. An electrochemical fabrication procedure to etch the tips is used to yield reproducible sub-100-nm apex. We also study electron t...

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Bibliographic Details
Authors: Rubio Bollinger, Gabino, Castellanos-Gomez, Andres, Bilan, Ştefan, Zotti, Linda Ángela, Arroyo, Carlos R., Agrait de la Puente, Mario Nicolás, Cuevas Rodríguez, Juan Carlos
Format: article
Publication Date:2012
Country:España
Institution:Universidad Autónoma de Madrid
Repository:Biblos-e Archivo. Repositorio Institucional de la UAM
Language:English
OAI Identifier:oai:repositorio.uam.es:10486/664624
Online Access:http://hdl.handle.net/10486/664624
https://dx.doi.org/10.1186/1556-276X-7-254
Access Level:Open access
Keyword:Carbon electrodes
Carbon electronics
Carbon tip
Quartz tuning fork
Single-molecule junction
STM break junction
Física
Description
Summary:We fabricate and characterize carbon-fiber tips for their use in combined scanning tunneling and force microscopy based on piezoelectric quartz tuning fork force sensors. An electrochemical fabrication procedure to etch the tips is used to yield reproducible sub-100-nm apex. We also study electron transport through single-molecule junctions formed by a single octanethiol molecule bonded by the thiol anchoring group to a gold electrode and linked to a carbon tip by the methyl group. We observe the presence of conductance plateaus during the stretching of the molecular bridge, which is the signature of the formation of a molecular junction