Gold and silver complexes of methylenebis(dialkyldithiocarbamates) and the X-ray structure of CH2[S2CN(CH2Ph)2]2

The coordination chemistry of CH2(S2CNR2)2 for R = Me, Et, n-Bu and benzyl with Au(I), Au(III) and Ag(I) is examined. The single crystal X-ray diffraction study of CH2[S2CN(CH2Ph)2]2 is described. Nineteen new complexes are characterized by IR, 1H, 19F, 31P (when appropriate) NMR, elemental analysis...

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Detalhes bibliográficos
Autores: Gimeno, M.C. [0000-0003-0553-0695], Jambrina, E., Laguna, A. [0000-0003-1984-7538], Laguna, M. [0000-0002-5801-3352], Murray, H.H., Terroba, R.
Formato: artículo
Estado:Versión publicada
Fecha de publicación:1996
País:España
Recursos:Universidad de La Rioja (UR)
Repositorio:RIUR. Repositorio Institucional de la Universidad de La Rioja
OAI Identifier:oai:portal.dialnet.es:doc/5bbc6850b750603269e80694
Acesso em linha:https://investigacion.unirioja.es/documentos/5bbc6850b750603269e80694
Access Level:acceso abierto
Palavra-chave:Crystal structures
Dithiocarbamato complexes
Gold complexes
Silver complexes
Descrição
Resumo:The coordination chemistry of CH2(S2CNR2)2 for R = Me, Et, n-Bu and benzyl with Au(I), Au(III) and Ag(I) is examined. The single crystal X-ray diffraction study of CH2[S2CN(CH2Ph)2]2 is described. Nineteen new complexes are characterized by IR, 1H, 19F, 31P (when appropriate) NMR, elemental analysis, mass spectra (FAB) and conductivity measurements. Neutral and cationic mono- and dinuclear species have been synthesized. The coordination chemistry of CH2(S2CNR2)2 is via the C=S functionality.