Development of advanced analytical methodologies based on gas chromatography coupled to mass spectometry for the determination of pops and vocs in the food and environmental field

The work in this thesis has been clearly divided into three parts: In the first part, efforts were directed to obtaining a trace level quantification method for halogenated flame retardants using high-volume injections and gas chromatography coupled to GC-MS/MS tandem mass spectrometry. In the secon...

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Autor: Sales Martínez, Carlos
Tipo de recurso: tesis doctoral
Estado:Versión publicada
Fecha de publicación:2019
País:España
Institución:CBUC, CESCA
Repositorio:TDR. Tesis Doctorales en Red
OAI Identifier:oai:www.tdx.cat:10803/668939
Acceso en línea:http://hdl.handle.net/10803/668939
http://dx.doi.org/10.6035/14104.2019.177055
Access Level:acceso abierto
Palabra clave:Gas Chromatography
Volatiles
Pollutants
Mass Spectrometry
Purge and Trap
Metabolomics
Ciències naturals, químiques, físiques i matemàtiques
543
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spelling Development of advanced analytical methodologies based on gas chromatography coupled to mass spectometry for the determination of pops and vocs in the food and environmental fieldSales Martínez, CarlosGas ChromatographyVolatilesPollutantsMass SpectrometryPurge and TrapMetabolomicsCiències naturals, químiques, físiques i matemàtiques543The work in this thesis has been clearly divided into three parts: In the first part, efforts were directed to obtaining a trace level quantification method for halogenated flame retardants using high-volume injections and gas chromatography coupled to GC-MS/MS tandem mass spectrometry. In the second part, the potential of the GC-MS / MS technique was evaluated together with the new atmospheric pressure chemical ionization source (APCI) for the quantification of PBDEs, NBFRs (including hexabromocyclododecane (HBCD)) and DL-PCBs at trace levels in food and environmental samples. In the third part, two untargeted analytical methodologies by GC-MS were developed as complementary tools to the PANEL TEST for the classification of olive oil samples according to their quality.El trabajo en la presente tesis se ha dividido claramente en tres partes: En la primera parte, los esfuerzos se dirigieron a la obtención de un método de cuantificación a nivel de trazas para retardantes de llama halogenados utilizando inyecciones de gran volumen y cromatografía de gases acoplada a espectrometría de masas en tándem GC-MS/MS. En la segunda parte, se evaluó el potencial de la técnica GC-MS/MS junto con la nueva fuente de ionización química a presión atmosférica (APCI) para la cuantificación de PBDEs, NBFRs (incluido el hexabromociclododecano (HBCD)) y DL-PCBs a niveles de traza en alimentos y muestras ambientales. En la tercera parte, se desarrollaron dos metodologías de análisis no dirigido por GC-MS como herramientas complementarias de la PRUEBA DE PANEL para la clasificación del aceite de oliva de acuerdo a su calidad.Programa de Doctorat en CiènciesUniversitat Jaume IBeltrán Arandes, JoaquínPortolés Nicolau, TaniaCovaci, AdrianUniversitat Jaume I. Escola de Doctorat202020202019info:eu-repo/semantics/doctoralThesisinfo:eu-repo/semantics/publishedVersion323 p.application/pdfapplication/pdfhttp://hdl.handle.net/10803/668939http://dx.doi.org/10.6035/14104.2019.177055TDX (Tesis Doctorals en Xarxa)reponame:TDR. Tesis Doctorales en Redinstname:CBUC, CESCAInglésL'accés als continguts d'aquesta tesi queda condicionat a l'acceptació de les condicions d'ús establertes per la següent llicència Creative Commons: http://creativecommons.org/licenses/by-nc-sa/4.0/http://creativecommons.org/licenses/by-nc-sa/4.0/info:eu-repo/semantics/openAccessoai:www.tdx.cat:10803/6689392026-06-14T12:46:07Z
dc.title.none.fl_str_mv Development of advanced analytical methodologies based on gas chromatography coupled to mass spectometry for the determination of pops and vocs in the food and environmental field
title Development of advanced analytical methodologies based on gas chromatography coupled to mass spectometry for the determination of pops and vocs in the food and environmental field
spellingShingle Development of advanced analytical methodologies based on gas chromatography coupled to mass spectometry for the determination of pops and vocs in the food and environmental field
Sales Martínez, Carlos
Gas Chromatography
Volatiles
Pollutants
Mass Spectrometry
Purge and Trap
Metabolomics
Ciències naturals, químiques, físiques i matemàtiques
543
title_short Development of advanced analytical methodologies based on gas chromatography coupled to mass spectometry for the determination of pops and vocs in the food and environmental field
title_full Development of advanced analytical methodologies based on gas chromatography coupled to mass spectometry for the determination of pops and vocs in the food and environmental field
title_fullStr Development of advanced analytical methodologies based on gas chromatography coupled to mass spectometry for the determination of pops and vocs in the food and environmental field
title_full_unstemmed Development of advanced analytical methodologies based on gas chromatography coupled to mass spectometry for the determination of pops and vocs in the food and environmental field
title_sort Development of advanced analytical methodologies based on gas chromatography coupled to mass spectometry for the determination of pops and vocs in the food and environmental field
dc.creator.none.fl_str_mv Sales Martínez, Carlos
author Sales Martínez, Carlos
author_facet Sales Martínez, Carlos
author_role author
dc.contributor.none.fl_str_mv Beltrán Arandes, Joaquín
Portolés Nicolau, Tania
Covaci, Adrian
Universitat Jaume I. Escola de Doctorat
dc.subject.none.fl_str_mv Gas Chromatography
Volatiles
Pollutants
Mass Spectrometry
Purge and Trap
Metabolomics
Ciències naturals, químiques, físiques i matemàtiques
543
topic Gas Chromatography
Volatiles
Pollutants
Mass Spectrometry
Purge and Trap
Metabolomics
Ciències naturals, químiques, físiques i matemàtiques
543
description The work in this thesis has been clearly divided into three parts: In the first part, efforts were directed to obtaining a trace level quantification method for halogenated flame retardants using high-volume injections and gas chromatography coupled to GC-MS/MS tandem mass spectrometry. In the second part, the potential of the GC-MS / MS technique was evaluated together with the new atmospheric pressure chemical ionization source (APCI) for the quantification of PBDEs, NBFRs (including hexabromocyclododecane (HBCD)) and DL-PCBs at trace levels in food and environmental samples. In the third part, two untargeted analytical methodologies by GC-MS were developed as complementary tools to the PANEL TEST for the classification of olive oil samples according to their quality.
publishDate 2019
dc.date.none.fl_str_mv 2019
2020
2020
dc.type.none.fl_str_mv info:eu-repo/semantics/doctoralThesis
info:eu-repo/semantics/publishedVersion
format doctoralThesis
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/10803/668939
http://dx.doi.org/10.6035/14104.2019.177055
url http://hdl.handle.net/10803/668939
http://dx.doi.org/10.6035/14104.2019.177055
dc.language.none.fl_str_mv Inglés
language_invalid_str_mv Inglés
dc.rights.none.fl_str_mv http://creativecommons.org/licenses/by-nc-sa/4.0/
info:eu-repo/semantics/openAccess
rights_invalid_str_mv http://creativecommons.org/licenses/by-nc-sa/4.0/
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv 323 p.
application/pdf
application/pdf
dc.publisher.none.fl_str_mv Universitat Jaume I
publisher.none.fl_str_mv Universitat Jaume I
dc.source.none.fl_str_mv TDX (Tesis Doctorals en Xarxa)
reponame:TDR. Tesis Doctorales en Red
instname:CBUC, CESCA
instname_str CBUC, CESCA
reponame_str TDR. Tesis Doctorales en Red
collection TDR. Tesis Doctorales en Red
repository.name.fl_str_mv
repository.mail.fl_str_mv
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score 15,300719

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