Transient liquid assisted growth of superconducting YBa2Cu3O7−x films based on pulsed laser deposition

We investigated the integration of transient liquid-assisted growth (TLAG) approach for epitaxial YBa2Cu3O7−x (YBCO) films by physical deposition methodologies (pulsed laser deposition (PLD)), as an additional opportunity for high-throughput growth of YBCO. As a prerequisite, highly flat and amorpho...

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Autores: Queraltó, Albert, Sieger, Max, Gupta, Kapil, Meledin, Alexander, Barusco, Pedro, Saltarelli, Lavinia, Palau, Mariona García de, Granados, Xavier, Obradors, Xavier, Puig Molina, Teresa
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2023
País:España
Institución:Consejo Superior de Investigaciones Científicas (CSIC)
Repositorio:DIGITAL.CSIC. Repositorio Institucional del CSIC
OAI Identifier:oai:digital.csic.es:10261/287237
Acceso en línea:http://hdl.handle.net/10261/287237
https://api.elsevier.com/content/abstract/scopus_id/85145351342
Access Level:acceso abierto
Palabra clave:Cuprate superconductors
Pulsed laser deposition
Superconducting materials
Transient liquid assisted growth
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dc.title.none.fl_str_mv Transient liquid assisted growth of superconducting YBa2Cu3O7−x films based on pulsed laser deposition
title Transient liquid assisted growth of superconducting YBa2Cu3O7−x films based on pulsed laser deposition
spellingShingle Transient liquid assisted growth of superconducting YBa2Cu3O7−x films based on pulsed laser deposition
Queraltó, Albert
Cuprate superconductors
Pulsed laser deposition
Superconducting materials
Transient liquid assisted growth
title_short Transient liquid assisted growth of superconducting YBa2Cu3O7−x films based on pulsed laser deposition
title_full Transient liquid assisted growth of superconducting YBa2Cu3O7−x films based on pulsed laser deposition
title_fullStr Transient liquid assisted growth of superconducting YBa2Cu3O7−x films based on pulsed laser deposition
title_full_unstemmed Transient liquid assisted growth of superconducting YBa2Cu3O7−x films based on pulsed laser deposition
title_sort Transient liquid assisted growth of superconducting YBa2Cu3O7−x films based on pulsed laser deposition
dc.creator.none.fl_str_mv Queraltó, Albert
Sieger, Max
Gupta, Kapil
Meledin, Alexander
Barusco, Pedro
Saltarelli, Lavinia
Palau, Mariona García de
Granados, Xavier
Obradors, Xavier
Puig Molina, Teresa
author Queraltó, Albert
author_facet Queraltó, Albert
Sieger, Max
Gupta, Kapil
Meledin, Alexander
Barusco, Pedro
Saltarelli, Lavinia
Palau, Mariona García de
Granados, Xavier
Obradors, Xavier
Puig Molina, Teresa
author_role author
author2 Sieger, Max
Gupta, Kapil
Meledin, Alexander
Barusco, Pedro
Saltarelli, Lavinia
Palau, Mariona García de
Granados, Xavier
Obradors, Xavier
Puig Molina, Teresa
author2_role author
author
author
author
author
author
author
author
author
dc.contributor.none.fl_str_mv European Research Council
European Cooperation in Science and Technology
Ministerio de Economía y Competitividad (España)
Ministerio de Ciencia, Innovación y Universidades (España)
Ministerio de Ciencia e Innovación (España)
Generalitat de Catalunya
Gupta, Kapil [0000-0002-4826-6620]
Meledin, Alexander [0000-0002-3200-0553]
Obradors, Xavier [0000-0003-4592-7718]
Consejo Superior de Investigaciones Científicas [https://ror.org/02gfc7t72]
dc.subject.none.fl_str_mv Cuprate superconductors
Pulsed laser deposition
Superconducting materials
Transient liquid assisted growth
topic Cuprate superconductors
Pulsed laser deposition
Superconducting materials
Transient liquid assisted growth
description We investigated the integration of transient liquid-assisted growth (TLAG) approach for epitaxial YBa2Cu3O7−x (YBCO) films by physical deposition methodologies (pulsed laser deposition (PLD)), as an additional opportunity for high-throughput growth of YBCO. As a prerequisite, highly flat and amorphous YBCO precursor films were deposited by PLD at temperatures below 400 °C on single-crystalline SrTiO3 (STO) and LaMnO3 (LMO)/STO, as well as industrial coated conductor architectures. Contrary to TLAG based on chemical solution deposition, where BaCO3 elimination is a key factor for the YBCO growth, TLAG-PLD growth is controlled by the transformation of Ba-Cu-O (s) to a transient liquid. High-quality c-axis YBCO films were successfully grown on different substrates, as demonstrated by high-resolution x-ray diffraction and transmission electron microscopy. In-situ resistance measurements revealed that the growth rates around 1000 nm s−1 can be achieved, outperforming the capabilities of standard PLD growth of REBa2Cu3O7 films by few orders of magnitude. Experimental conditions such as temperature, oxygen partial pressure, and heating ramp, were optimized to obtain critical temperature (T c) values up to 90 K. Critical current densities of 15 MA cm−2 at 5 K and 1.7 MA cm−2 at 77 K were obtained for YBCO films of 450 nm on LMO/STO.
publishDate 2023
dc.date.none.fl_str_mv 2023
2023
2023
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Publisher's version
info:eu-repo/semantics/publishedVersion
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/10261/287237
https://api.elsevier.com/content/abstract/scopus_id/85145351342
url http://hdl.handle.net/10261/287237
https://api.elsevier.com/content/abstract/scopus_id/85145351342
dc.language.none.fl_str_mv Inglés
language_invalid_str_mv Inglés
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info:eu-repo/grantAgreement/EC/H2020/669504
info:eu-repo/grantAgreement/EC/H2020/874964
info:eu-repo/grantAgreement/EC/HE/101081998
info:eu-repo/grantAgreement/MINECO//SEV-2015-0496
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Superconductor Science and Technology
http://dx.doi.org/10.1088/1361-6668/acaad3
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dc.publisher.none.fl_str_mv Institute of Physics Publishing
publisher.none.fl_str_mv Institute of Physics Publishing
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spelling Transient liquid assisted growth of superconducting YBa2Cu3O7−x films based on pulsed laser depositionQueraltó, AlbertSieger, MaxGupta, KapilMeledin, AlexanderBarusco, PedroSaltarelli, LaviniaPalau, Mariona García deGranados, XavierObradors, XavierPuig Molina, TeresaCuprate superconductorsPulsed laser depositionSuperconducting materialsTransient liquid assisted growthWe investigated the integration of transient liquid-assisted growth (TLAG) approach for epitaxial YBa2Cu3O7−x (YBCO) films by physical deposition methodologies (pulsed laser deposition (PLD)), as an additional opportunity for high-throughput growth of YBCO. As a prerequisite, highly flat and amorphous YBCO precursor films were deposited by PLD at temperatures below 400 °C on single-crystalline SrTiO3 (STO) and LaMnO3 (LMO)/STO, as well as industrial coated conductor architectures. Contrary to TLAG based on chemical solution deposition, where BaCO3 elimination is a key factor for the YBCO growth, TLAG-PLD growth is controlled by the transformation of Ba-Cu-O (s) to a transient liquid. High-quality c-axis YBCO films were successfully grown on different substrates, as demonstrated by high-resolution x-ray diffraction and transmission electron microscopy. In-situ resistance measurements revealed that the growth rates around 1000 nm s−1 can be achieved, outperforming the capabilities of standard PLD growth of REBa2Cu3O7 films by few orders of magnitude. Experimental conditions such as temperature, oxygen partial pressure, and heating ramp, were optimized to obtain critical temperature (T c) values up to 90 K. Critical current densities of 15 MA cm−2 at 5 K and 1.7 MA cm−2 at 77 K were obtained for YBCO films of 450 nm on LMO/STO.The authors acknowledge European Research Council for the ULTRASUPERTAPE project (ERC-2014-ADG-669504), IMPACT project (ERC-2019-PoC-874964) and SMS-INKS project (ERC-2022-PoC-101081998), as well as the EU COST actions CA16218 (NANOCOHYBRI), CA20116 (OPERA) and CA21144 (SUPERQUMAP). We also thank financial support from the Spanish Ministry of Economy and Competitiveness, and Spanish Ministry of Science, Innovation and Universities through the 'Severo Ochoa' Programme for Centres of Excellence in R&D (SEV-2015-0496 and CEX2019-000917-S), FUNFUTURE-FIP-2020-DATOPTICON, SUPERENERTECH project (PID2021-127297OB-C21), and SUMATE project (RTI2018-095853-B-C21, co-financed by the European Regional Development Fund). We also acknowledge support from the Catalan Government with 2017-SGR-1519 and the Catalan energy network XRE4S (2018 XARDI 00002). A Q thanks the Spanish Ministry of Science, Innovation and Universities for his 'Juan de la Cierva' postdoctoral fellowship (Grant No. IJC2018-035034-I). L S acknowledges financial support from Spanish Ministry of Science, Innovation and Universities through the FPI grants PRE2019-090621. Dr Silvia Rasi and Dr Roxana Vlad are thanked for fruitful discussions. We acknowledge the Scientific Services at ICMAB and ICN2 Electron Microscopy Division. Authors also acknowledge the use of instrumentation as well as the technical advice provided by the National Facility ELECMI ICTS, node 'Laboratorio de Microscopías Avanzadas' at University of Zaragoza. SuNAM Co. is acknowledged for providing metallic substrates.With funding from the Spanish government through the ‘Severo Ochoa Centre of Excellence’ accreditation (CEX2019-000917-S).Peer reviewedInstitute of Physics PublishingEuropean Research CouncilEuropean Cooperation in Science and TechnologyMinisterio de Economía y Competitividad (España)Ministerio de Ciencia, Innovación y Universidades (España)Ministerio de Ciencia e Innovación (España)Generalitat de CatalunyaGupta, Kapil [0000-0002-4826-6620]Meledin, Alexander [0000-0002-3200-0553]Obradors, Xavier [0000-0003-4592-7718]Consejo Superior de Investigaciones Científicas [https://ror.org/02gfc7t72]202320232023info:eu-repo/semantics/articlehttp://purl.org/coar/resource_type/c_6501Publisher's versioninfo:eu-repo/semantics/publishedVersionhttp://hdl.handle.net/10261/287237https://api.elsevier.com/content/abstract/scopus_id/85145351342reponame:DIGITAL.CSIC. 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