Structural and surface considerations on Mo/ZSM-5 systems for methane dehydroaromatization reaction

We have prepared a series of Mo/ZSM-5 systems by impregnation method with different metal loading. The optimum performance has been attained for 4% metal loading, yielding to ca. 2 mmolbenzene/gcat at the end of the reaction. The obtained catalysts were widely structural and surface characterized. A...

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Detalles Bibliográficos
Autores: López Martín, Ángeles, Caballero Martínez, Alfonso, Colón, Gerardo
Tipo de recurso: artículo
Estado:Versión aceptada para publicación
Fecha de publicación:2020
País:España
Institución:Universidad de Sevilla (US)
Repositorio:idUS. Depósito de Investigación de la Universidad de Sevilla
OAI Identifier:oai:idus.us.es:11441/183498
Acceso en línea:https://hdl.handle.net/11441/183498
https://doi.org/10.1016/j.mcat.2020.110787
Access Level:acceso abierto
Palabra clave:Molybdenum
ZSM-5
Methane
Dehydroaromatization
Descripción
Sumario:We have prepared a series of Mo/ZSM-5 systems by impregnation method with different metal loading. The optimum performance has been attained for 4% metal loading, yielding to ca. 2 mmolbenzene/gcat at the end of the reaction. The obtained catalysts were widely structural and surface characterized. As Mo content increases, the surface feature of the support is affected specially its mesoporosity. It has been stated the enormous complexity of Mo species present in the studied system. In situ characterization by XPS reveals different reduction and carburization behaviour depending on the Mo content.