Unraveling the Mo/HZSM-5 Reduction Pre-treatment Effect on Methane Dehydroaromatization Reaction

Reduction pre-treatment at different temperatures were performed over Mo/HZSM-5 system before methane dehydroaromatiztion reaction. We have shown the crucial effect of reduction temperature on the final catalytic performance. Outstanding improvement in the aromatics conversion has been attained. Thu...

Descripción completa

Detalles Bibliográficos
Autores: López Martín, Ángeles, Caballero Martínez, Alfonso, Colón, Gerardo
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2022
País:España
Institución:Universidad de Sevilla (US)
Repositorio:idUS. Depósito de Investigación de la Universidad de Sevilla
OAI Identifier:oai:idus.us.es:11441/154362
Acceso en línea:https://hdl.handle.net/11441/154362
https://doi.org/10.1016/j.apcatb.2022.121382
Access Level:acceso abierto
Palabra clave:Dehydroaromatization
Methane
Molybdenum
Pre-treatment
ZSM-5
Descripción
Sumario:Reduction pre-treatment at different temperatures were performed over Mo/HZSM-5 system before methane dehydroaromatiztion reaction. We have shown the crucial effect of reduction temperature on the final catalytic performance. Outstanding improvement in the aromatics conversion has been attained. Thus, H2 formation form methane cracking reaction seems to be hindered for pre-treated catalysts. As a consequence, the deposition of coke in these samples appeared also notably suppressed. The optimum performance has been achieved for reduction pre-treatment at 550 ºC. For this temperature, we have observed that the fraction of reduced Mo species is higher.