Improved stability and spectral quality in ex situ dissolution DNP using an improved transfer device

Dissolution dynamic nuclear polarization (DNP) has become one of the predominant implementations for DNP. However, the technical implementation of transferring the sample from the polarizer to the nuclear magnetic resonance (NMR) system remains challenging. There is a need for additional technical o...

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Autores: Katsikis, Sotirios, Marín Montesinos, Ildefonso, Pons Vallès, Miquel, Ludwig, Christian, Günther, Ulrich L.
Tipo de recurso: artículo
Estado:Versión aceptada para publicación
Fecha de publicación:2015
País:España
Institución:Universidad de Barcelona
Repositorio:Dipòsit Digital de la UB
OAI Identifier:oai:diposit.ub.edu:2445/138570
Acceso en línea:https://hdl.handle.net/2445/138570
Access Level:acceso abierto
Palabra clave:Espectroscòpia de ressonància magnètica nuclear
Polarització (Física nuclear)
Nuclear magnetic resonance spectroscopy
Polarization (Nuclear physics)
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spelling Improved stability and spectral quality in ex situ dissolution DNP using an improved transfer deviceKatsikis, SotiriosMarín Montesinos, IldefonsoPons Vallès, MiquelLudwig, ChristianGünther, Ulrich L.Espectroscòpia de ressonància magnètica nuclearPolarització (Física nuclear)Nuclear magnetic resonance spectroscopyPolarization (Nuclear physics)Dissolution dynamic nuclear polarization (DNP) has become one of the predominant implementations for DNP. However, the technical implementation of transferring the sample from the polarizer to the nuclear magnetic resonance (NMR) system remains challenging. There is a need for additional technical optimizations in order to use dissolution DNP for biochemical and chemical applications. Here we show how a newly designed pressure dissolution kit considerably improves spectral quality and stability by enabling highly reliable and fast sample transfer to the NMR system.Springer Verlag2015info:eu-repo/semantics/articleinfo:eu-repo/semantics/acceptedVersionapplication/pdfhttps://hdl.handle.net/2445/138570Articles publicats en revistes (Química Inorgànica i Orgànica)reponame:Dipòsit Digital de la UBinstname:Universidad de BarcelonaInglésVersió postprint del document publicat a: https://doi.org/10.1007/s00723-015-0680-5Applied Magnetic Resonance, 2015, vol. 46, num. 7, p. 723-729https://doi.org/10.1007/s00723-015-0680-5 info:eu-repo/grantAgreement/EC/FP7/261863/EU//BIO-NMR(c) Springer Verlag, 2015info:eu-repo/semantics/openAccessoai:diposit.ub.edu:2445/1385702026-05-27T06:46:51Z
dc.title.none.fl_str_mv Improved stability and spectral quality in ex situ dissolution DNP using an improved transfer device
title Improved stability and spectral quality in ex situ dissolution DNP using an improved transfer device
spellingShingle Improved stability and spectral quality in ex situ dissolution DNP using an improved transfer device
Katsikis, Sotirios
Espectroscòpia de ressonància magnètica nuclear
Polarització (Física nuclear)
Nuclear magnetic resonance spectroscopy
Polarization (Nuclear physics)
title_short Improved stability and spectral quality in ex situ dissolution DNP using an improved transfer device
title_full Improved stability and spectral quality in ex situ dissolution DNP using an improved transfer device
title_fullStr Improved stability and spectral quality in ex situ dissolution DNP using an improved transfer device
title_full_unstemmed Improved stability and spectral quality in ex situ dissolution DNP using an improved transfer device
title_sort Improved stability and spectral quality in ex situ dissolution DNP using an improved transfer device
dc.creator.none.fl_str_mv Katsikis, Sotirios
Marín Montesinos, Ildefonso
Pons Vallès, Miquel
Ludwig, Christian
Günther, Ulrich L.
author Katsikis, Sotirios
author_facet Katsikis, Sotirios
Marín Montesinos, Ildefonso
Pons Vallès, Miquel
Ludwig, Christian
Günther, Ulrich L.
author_role author
author2 Marín Montesinos, Ildefonso
Pons Vallès, Miquel
Ludwig, Christian
Günther, Ulrich L.
author2_role author
author
author
author
dc.subject.none.fl_str_mv Espectroscòpia de ressonància magnètica nuclear
Polarització (Física nuclear)
Nuclear magnetic resonance spectroscopy
Polarization (Nuclear physics)
topic Espectroscòpia de ressonància magnètica nuclear
Polarització (Física nuclear)
Nuclear magnetic resonance spectroscopy
Polarization (Nuclear physics)
description Dissolution dynamic nuclear polarization (DNP) has become one of the predominant implementations for DNP. However, the technical implementation of transferring the sample from the polarizer to the nuclear magnetic resonance (NMR) system remains challenging. There is a need for additional technical optimizations in order to use dissolution DNP for biochemical and chemical applications. Here we show how a newly designed pressure dissolution kit considerably improves spectral quality and stability by enabling highly reliable and fast sample transfer to the NMR system.
publishDate 2015
dc.date.none.fl_str_mv 2015
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/acceptedVersion
format article
status_str acceptedVersion
dc.identifier.none.fl_str_mv https://hdl.handle.net/2445/138570
url https://hdl.handle.net/2445/138570
dc.language.none.fl_str_mv Inglés
language_invalid_str_mv Inglés
dc.relation.none.fl_str_mv Versió postprint del document publicat a: https://doi.org/10.1007/s00723-015-0680-5
Applied Magnetic Resonance, 2015, vol. 46, num. 7, p. 723-729
https://doi.org/10.1007/s00723-015-0680-5
 info:eu-repo/grantAgreement/EC/FP7/261863/EU//BIO-NMR
dc.rights.none.fl_str_mv (c) Springer Verlag, 2015
info:eu-repo/semantics/openAccess
rights_invalid_str_mv (c) Springer Verlag, 2015
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
dc.publisher.none.fl_str_mv Springer Verlag
publisher.none.fl_str_mv Springer Verlag
dc.source.none.fl_str_mv Articles publicats en revistes (Química Inorgànica i Orgànica)
reponame:Dipòsit Digital de la UB
instname:Universidad de Barcelona
instname_str Universidad de Barcelona
reponame_str Dipòsit Digital de la UB
collection Dipòsit Digital de la UB
repository.name.fl_str_mv
repository.mail.fl_str_mv
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score 15.300719

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