Microwave assisted synthesis of polynuclear Ni(II) complexes

In this paper we test a solvent-free microwave assisted synthesis method with a known Ni7 complex, [Ni7(chp)12(OH)2(CH3OH)6] (2), and then extended the method to a more complex ligand system. We prepare two new trinuclear Ni(II) complexes ([Ni3(chp)4(tBuSALOH)2(MeOH)5] (4) and [Ni3(chp)4(iPrSALOH)2(...

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Authors: Rosado Piquer, Lidia, Sañudo Zotes, Eva Carolina
Format: article
Status:Versión aceptada para publicación
Publication Date:2019
Country:España
Institution:Varias* (Consorci de Biblioteques Universitáries de Catalunya, Centre de Serveis Científics i Acadèmics de Catalunya)
Repository:Recercat. Dipósit de la Recerca de Catalunya
OAI Identifier:oai:recercat.cat:2445/139420
Online Access:https://hdl.handle.net/2445/139420
Access Level:Open access
Keyword:Complexos metàl·lics
Propietats magnètiques
Metal complexes
Magnetic properties
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spelling Microwave assisted synthesis of polynuclear Ni(II) complexesRosado Piquer, LidiaSañudo Zotes, Eva CarolinaComplexos metàl·licsPropietats magnètiquesMetal complexesMagnetic propertiesIn this paper we test a solvent-free microwave assisted synthesis method with a known Ni7 complex, [Ni7(chp)12(OH)2(CH3OH)6] (2), and then extended the method to a more complex ligand system. We prepare two new trinuclear Ni(II) complexes ([Ni3(chp)4(tBuSALOH)2(MeOH)5] (4) and [Ni3(chp)4(iPrSALOH)2(MeOH)6] (5)) and report here their characterization and magnetic properties.Elsevier Ltd2019202120192019info:eu-repo/semantics/articleinfo:eu-repo/semantics/acceptedVersion7 p.application/pdfhttps://hdl.handle.net/2445/139420Articles publicats en revistes (Química Inorgànica i Orgànica)reponame:Recercat. Dipósit de la Recerca de Catalunyainstname:Varias* (Consorci de Biblioteques Universitáries de Catalunya, Centre de Serveis Científics i Acadèmics de Catalunya)InglésVersió postprint del document publicat a: https://doi.org/10.1016/j.poly.2019.05.011Polyhedron, 2019, vol. 169, p. 195-201https://doi.org/10.1016/j.poly.2019.05.011cc-by-nc-nd (c) Elsevier Ltd, 2019http://creativecommons.org/licenses/by-nc-nd/3.0/esinfo:eu-repo/semantics/openAccessoai:recercat.cat:2445/1394202026-05-29T05:05:01Z
dc.title.none.fl_str_mv Microwave assisted synthesis of polynuclear Ni(II) complexes
title Microwave assisted synthesis of polynuclear Ni(II) complexes
spellingShingle Microwave assisted synthesis of polynuclear Ni(II) complexes
Rosado Piquer, Lidia
Complexos metàl·lics
Propietats magnètiques
Metal complexes
Magnetic properties
title_short Microwave assisted synthesis of polynuclear Ni(II) complexes
title_full Microwave assisted synthesis of polynuclear Ni(II) complexes
title_fullStr Microwave assisted synthesis of polynuclear Ni(II) complexes
title_full_unstemmed Microwave assisted synthesis of polynuclear Ni(II) complexes
title_sort Microwave assisted synthesis of polynuclear Ni(II) complexes
dc.creator.none.fl_str_mv Rosado Piquer, Lidia
Sañudo Zotes, Eva Carolina
author Rosado Piquer, Lidia
author_facet Rosado Piquer, Lidia
Sañudo Zotes, Eva Carolina
author_role author
author2 Sañudo Zotes, Eva Carolina
author2_role author
dc.subject.none.fl_str_mv Complexos metàl·lics
Propietats magnètiques
Metal complexes
Magnetic properties
topic Complexos metàl·lics
Propietats magnètiques
Metal complexes
Magnetic properties
description In this paper we test a solvent-free microwave assisted synthesis method with a known Ni7 complex, [Ni7(chp)12(OH)2(CH3OH)6] (2), and then extended the method to a more complex ligand system. We prepare two new trinuclear Ni(II) complexes ([Ni3(chp)4(tBuSALOH)2(MeOH)5] (4) and [Ni3(chp)4(iPrSALOH)2(MeOH)6] (5)) and report here their characterization and magnetic properties.
publishDate 2019
dc.date.none.fl_str_mv 2019
2019
2019
2021
dc.type.none.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/acceptedVersion
format article
status_str acceptedVersion
dc.identifier.none.fl_str_mv https://hdl.handle.net/2445/139420
url https://hdl.handle.net/2445/139420
dc.language.none.fl_str_mv Inglés
language_invalid_str_mv Inglés
dc.relation.none.fl_str_mv Versió postprint del document publicat a: https://doi.org/10.1016/j.poly.2019.05.011
Polyhedron, 2019, vol. 169, p. 195-201
https://doi.org/10.1016/j.poly.2019.05.011
dc.rights.none.fl_str_mv cc-by-nc-nd (c) Elsevier Ltd, 2019
http://creativecommons.org/licenses/by-nc-nd/3.0/es
info:eu-repo/semantics/openAccess
rights_invalid_str_mv cc-by-nc-nd (c) Elsevier Ltd, 2019
http://creativecommons.org/licenses/by-nc-nd/3.0/es
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv 7 p.
application/pdf
dc.publisher.none.fl_str_mv Elsevier Ltd
publisher.none.fl_str_mv Elsevier Ltd
dc.source.none.fl_str_mv Articles publicats en revistes (Química Inorgànica i Orgànica)
reponame:Recercat. Dipósit de la Recerca de Catalunya
instname:Varias* (Consorci de Biblioteques Universitáries de Catalunya, Centre de Serveis Científics i Acadèmics de Catalunya)
instname_str Varias* (Consorci de Biblioteques Universitáries de Catalunya, Centre de Serveis Científics i Acadèmics de Catalunya)
reponame_str Recercat. Dipósit de la Recerca de Catalunya
collection Recercat. Dipósit de la Recerca de Catalunya
repository.name.fl_str_mv
repository.mail.fl_str_mv
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score 15.811543

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