Optimizing Thermoelectric Properties through Compositional Engineering in Ag-Deficient AgSbTe<sub>2</sub> Synthesized by Arc Melting

Thermoelectric materials offer a promising avenue for energy management, directly converting heat into electrical energy. Among them, AgSbTe2 has gained significant attention and continues to be a subject of research at further improving its thermoelectric performance and expanding its practical app...

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Detalles Bibliográficos
Autores: Prado Gonjal, Jesús de la Paz, García-Calvo, Elena, Gainza, Javier, Durá, Oscar J., Dejoie, Catherine, Nemes, Norbert Marcel, Martínez, José Luis, Alonso, José Antonio, Serrano-Sánchez, Federico
Tipo de recurso: artículo
Fecha de publicación:2024
País:España
Institución:Universidad Complutense de Madrid (UCM)
Repositorio:Docta Complutense
Idioma:inglés
OAI Identifier:oai:docta.ucm.es:20.500.14352/104910
Acceso en línea:https://hdl.handle.net/20.500.14352/104910
Access Level:acceso abierto
Palabra clave:54
thermeoelectrics
AgSbTe2
arc-melting
compositional engineering
Química
Física (Física)
Física del estado sólido
Cristalografía (Química)
23 Química
2210.28 Química del Estado Sólido
2207.09 Conversión de Energía
2211.04 Cristalografía
Descripción
Sumario:Thermoelectric materials offer a promising avenue for energy management, directly converting heat into electrical energy. Among them, AgSbTe2 has gained significant attention and continues to be a subject of research at further improving its thermoelectric performance and expanding its practical applications. This study focuses on Ag-deficient Ag0.7Sb1.12Te2 and Ag0.7Sb1.12Te1.95Se0.05 materials, examining the impact of compositional engineering within the AgSbTe2 thermoelectric system. These materials have been rapidly synthesized using an arc-melting technique, resulting in the production of dense nanostructured pellets. Detailed analysis through scanning electron microscopy (SEM) reveals the presence of a layered nanostructure, which significantly influences the thermoelectric properties of these materials. Synchrotron X-ray diffraction reveals significant changes in the lattice parameters and atomic displacement parameters (ADPs) that suggest a weakening of bond order in the structure. The thermoelectric characterization highlights the enhanced power factor of Ag-deficient materials that, combined with the low glass-like thermal conductivity, results in a significant improvement in the figure of merit, achieving zT values of 1.25 in Ag0.7Sb1.12Te2 and 1.01 in Ag0.7Sb1.12Te1.95Se0.05 at 750 K.