AFM assessment of the surface nano/microstructure on chemically damaged historical and model glasses

Surface chemical damage on selected historicalglasses from 13th to 19th centuries was evaluated by means of atomic force microscopy (AFM). Nano- and microstructure, roughness and topography of ancient glass samples have been compared with those of modelglasses prepared by conventional melting at the...

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Authors: Carmona, N., Kowal, Andrzej, Rincón López, Jesús María, Villegas Broncano, María Ángeles
Format: article
Status:Versión enviada para evaluación y publicación
Publication Date:2010
Country:España
Institution:Consejo Superior de Investigaciones Científicas (CSIC)
Repository:DIGITAL.CSIC. Repositorio Institucional del CSIC
OAI Identifier:oai:digital.csic.es:10261/55068
Online Access:http://hdl.handle.net/10261/55068
Access Level:Open access
Keyword:Glasses
Atomic force microscopy
Electron microscopy (SEM)
Corrosion
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spelling AFM assessment of the surface nano/microstructure on chemically damaged historical and model glassesCarmona, N.Kowal, AndrzejRincón López, Jesús MaríaVillegas Broncano, María ÁngelesGlassesAtomic force microscopyElectron microscopy (SEM)CorrosionSurface chemical damage on selected historicalglasses from 13th to 19th centuries was evaluated by means of atomic force microscopy (AFM). Nano- and microstructure, roughness and topography of ancient glass samples have been compared with those of modelglasses prepared by conventional melting at the laboratory with similar compositions to those most frequently found in historicalglass pieces. The results obtained allow discussing the chemical degradation mechanisms in terms of the acid and/or basic chemical attack carried out by the combination of gaseous pollutants and environmental humidity. Even though deep corrosion features escape to the observation order of magnitude of the AF microscope used, the AFM technique proves to be quite useful for the study and evaluation of the most common surface pathologies of historicalglasses with different compositions once submitted to natural weathering.NoElsevierConsejo Superior de Investigaciones Científicas [https://ror.org/02gfc7t72]201220122010info:eu-repo/semantics/articlehttp://purl.org/coar/resource_type/c_6501Preprintinfo:eu-repo/semantics/submittedVersionapplication/pdfhttp://hdl.handle.net/10261/55068reponame:DIGITAL.CSIC. Repositorio Institucional del CSICinstname:Consejo Superior de Investigaciones Científicas (CSIC)Ingléshttp://dx.doi.org/10.1016/j.matchemphys.2009.08.052Síinfo:eu-repo/semantics/openAccessoai:digital.csic.es:10261/550682026-05-22T06:33:51Z
dc.title.none.fl_str_mv AFM assessment of the surface nano/microstructure on chemically damaged historical and model glasses
title AFM assessment of the surface nano/microstructure on chemically damaged historical and model glasses
spellingShingle AFM assessment of the surface nano/microstructure on chemically damaged historical and model glasses
Carmona, N.
Glasses
Atomic force microscopy
Electron microscopy (SEM)
Corrosion
title_short AFM assessment of the surface nano/microstructure on chemically damaged historical and model glasses
title_full AFM assessment of the surface nano/microstructure on chemically damaged historical and model glasses
title_fullStr AFM assessment of the surface nano/microstructure on chemically damaged historical and model glasses
title_full_unstemmed AFM assessment of the surface nano/microstructure on chemically damaged historical and model glasses
title_sort AFM assessment of the surface nano/microstructure on chemically damaged historical and model glasses
dc.creator.none.fl_str_mv Carmona, N.
Kowal, Andrzej
Rincón López, Jesús María
Villegas Broncano, María Ángeles
author Carmona, N.
author_facet Carmona, N.
Kowal, Andrzej
Rincón López, Jesús María
Villegas Broncano, María Ángeles
author_role author
author2 Kowal, Andrzej
Rincón López, Jesús María
Villegas Broncano, María Ángeles
author2_role author
author
author
dc.contributor.none.fl_str_mv Consejo Superior de Investigaciones Científicas [https://ror.org/02gfc7t72]
dc.subject.none.fl_str_mv Glasses
Atomic force microscopy
Electron microscopy (SEM)
Corrosion
topic Glasses
Atomic force microscopy
Electron microscopy (SEM)
Corrosion
description Surface chemical damage on selected historicalglasses from 13th to 19th centuries was evaluated by means of atomic force microscopy (AFM). Nano- and microstructure, roughness and topography of ancient glass samples have been compared with those of modelglasses prepared by conventional melting at the laboratory with similar compositions to those most frequently found in historicalglass pieces. The results obtained allow discussing the chemical degradation mechanisms in terms of the acid and/or basic chemical attack carried out by the combination of gaseous pollutants and environmental humidity. Even though deep corrosion features escape to the observation order of magnitude of the AF microscope used, the AFM technique proves to be quite useful for the study and evaluation of the most common surface pathologies of historicalglasses with different compositions once submitted to natural weathering.
publishDate 2010
dc.date.none.fl_str_mv 2010
2012
2012
dc.type.none.fl_str_mv info:eu-repo/semantics/article
http://purl.org/coar/resource_type/c_6501
Preprint
info:eu-repo/semantics/submittedVersion
format article
status_str submittedVersion
dc.identifier.none.fl_str_mv http://hdl.handle.net/10261/55068
url http://hdl.handle.net/10261/55068
dc.language.none.fl_str_mv Inglés
language_invalid_str_mv Inglés
dc.relation.none.fl_str_mv http://dx.doi.org/10.1016/j.matchemphys.2009.08.052
Sí
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
dc.publisher.none.fl_str_mv Elsevier
publisher.none.fl_str_mv Elsevier
dc.source.none.fl_str_mv reponame:DIGITAL.CSIC. Repositorio Institucional del CSIC
instname:Consejo Superior de Investigaciones Científicas (CSIC)
instname_str Consejo Superior de Investigaciones Científicas (CSIC)
reponame_str DIGITAL.CSIC. Repositorio Institucional del CSIC
collection DIGITAL.CSIC. Repositorio Institucional del CSIC
repository.name.fl_str_mv
repository.mail.fl_str_mv
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score 15,811543

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