Synthesis and reactivity of a trigonal porous nanographene on a gold surface

The synthesis of porous nanographenes is a challenging task for solution chemistry, and thus, on-surface synthesis provides an alternative approach. Here, we report the synthesis of a triporous nanographene with 102 sp2 carbon atoms by combining solution and surface chemistry. The carbon skeleton wa...

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Detalles Bibliográficos
Autores: Zuzak, Rafał, Pozo Míguez, Iago, Engelund, Mads, García Lekue, Aran, Vilas Varela, Manuel, Alonso, José M., Szymonski, Marek, Guitián Rivera, Enrique, Pérez Meirás, María Dolores, Godlewski, Szymon, Peña Gil, Diego
Tipo de recurso: artículo
Fecha de publicación:2019
País:España
Institución:Universidad de Santiago de Compostela (USC)
Repositorio:Minerva. Repositorio Institucional de la Universidad de Santiago de Compostela
Idioma:inglés
OAI Identifier:oai:minerva.usc.gal:10347/21330
Acceso en línea:http://hdl.handle.net/10347/21330
Access Level:acceso abierto
Descripción
Sumario:The synthesis of porous nanographenes is a challenging task for solution chemistry, and thus, on-surface synthesis provides an alternative approach. Here, we report the synthesis of a triporous nanographene with 102 sp2 carbon atoms by combining solution and surface chemistry. The carbon skeleton was obtained by Pd-catalyzed cyclotrimerization of arynes in solution, while planarization of the molecule was achieved through two hierarchically organized on-surface cyclodehydrogenation reactions, intra- and inter-blade. Remarkably, the three non-planar [14]annulene pores of this nanographene further evolved at higher temperatures showing interesting intra-porous on-surface reactivity