Crystal structure and Hirshfeld surface analysis of diiodido{N'-[(E)-(phenyl)(pyridin-2-yl-κN)methylidene]pyridine-2-carbohydrazide-κ2 N',O}cadmium(II)

In each of the two independent molecules in the asymmetric unit of the title compound, [CdI2(C18H14N4O)], the N,O,N'-tridentate N'-[(E)-(phenyl)(pyridin-2-yl-κN)methylidene]pyridine-2-carbohydrazide ligand and two iodide anions form an I2NO pentacoordination sphere, with a distorted square...

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Detalles Bibliográficos
Autores: Atioglu, Zeliha, Akbari Afkhami, Farhad, Akkurt, Mehmet, Akbar Khandar, Ali, Choquesillo-Lazarte, Duane
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2019
País:España
Institución:Consejo Superior de Investigaciones Científicas (CSIC)
Repositorio:DIGITAL.CSIC. Repositorio Institucional del CSIC
OAI Identifier:oai:digital.csic.es:10261/204908
Acceso en línea:http://hdl.handle.net/10261/204908
Access Level:acceso abierto
Palabra clave:Crystal structures
Cadmium
Iodide
Descripción
Sumario:In each of the two independent molecules in the asymmetric unit of the title compound, [CdI2(C18H14N4O)], the N,O,N'-tridentate N'-[(E)-(phenyl)(pyridin-2-yl-κN)methylidene]pyridine-2-carbohydrazide ligand and two iodide anions form an I2NO pentacoordination sphere, with a distorted square-pyramidal geometry, with an I atom in the apical position. Both molecules feature an intramolecular N - H⋯N hydrogen bond. In the crystal, weak aromatic π-π stacking interactions [centroid-centroid separation = 3.830 (2) Å] link the molecules into dimers.