Insights into the occurrence and biotoxicity impact of zinc oxide nanoparticles within healthcare and sanitary products

The potential occurrence of zinc oxide nanoparticles (ZnONPs) within healthcare and sanitary products labelled as containing bulk ZnO has become an emerging issue, due to their controversial biotoxicity derived from their recently reported enzyme-like behaviour. To monitor and shed light on it, a mu...

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Detalles Bibliográficos
Autores: Sánchez Cachero, Armando, Bartolomé Díaz, Manuel, Fernández-Pacheco Rodríguez, Pilar, Arévalo Villena, María, Rodríguez Martín-Doimeadios, Rosa del Carmen, Villaseñor Llerena, María Jesús, Ríos Castro, Ángel
Tipo de recurso: artículo
Fecha de publicación:2026
País:España
Institución:Universidad de Castilla-La Mancha
Repositorio:RUIdeRA. Repositorio Institucional de la UCLM
OAI Identifier:oai:dnet:ruidera_____::59e81a227c4fa2567acb8230734959eb
Acceso en línea:https://doi.org/10.1016/j.talanta.2026.129922
https://www.sciencedirect.com/science/article/pii/S0039914026005783
https://hdl.handle.net/10578/48370
Access Level:acceso abierto
Palabra clave:Antimicrobial activity
Catalytic nanozymes
Nanobiotoxicity
Single particle inductively coupled plasma mass spectrometry
Zinc oxide nanoparticles
Descripción
Sumario:The potential occurrence of zinc oxide nanoparticles (ZnONPs) within healthcare and sanitary products labelled as containing bulk ZnO has become an emerging issue, due to their controversial biotoxicity derived from their recently reported enzyme-like behaviour. To monitor and shed light on it, a multidisciplinary approach has been devised in the present work. Firstly, biotoxicity tests of bulk ZnO and ZnONPs were performed on nine different microorganism strains (yeasts and bacteria), characteristic pathogen and commensal human microbiota inhabiting affected human tissues. Secondly, assorted commercial healthcare and sanitary products containing bulk ZnO (with undeclared ZnONPs) were analyzed by single particle inductively coupled plasma mass spectrometry (spICP-MS). With this aim, an ultrasonic probe-assisted extraction using Triton X-100 1% was applied, and commercial ZnONP powder was used as an internal quality control material. The evaluation of analytical performance features in terms of trueness (particle number concentration and equivalent size), precision, and limits of detection in size and concentration proves the suitability of the methodology regarding preservation of native size, size distribution, and number of NPs. Biotoxicity assays evidenced higher inhibition halos for ZnONPs than for bulk ZnO with a clear size-dependent NPs behaviour and substantial variability in bacterial susceptibility. Minimum inhibitory concentrations (MIC) needed to act on pathogens resulted clearly able to compromise commensal microbiota. Hence, the obtained findings reveal potential toxicity risks and the need to control them using appropriate tools, as some commercial samples presented ZnONP percentages outside of a safety scenario, as well as the advisability of reassessing the legal framework.