Supporting Information: Continuous microwave-assisted synthesis of silver nanoclusters confined in mesoporous SBA-15: Application in alkyne cyclizations

Optimization of heating time in batch synthesis (Figure S1); physical and geometrical parameters adopted for Comsol Multiphysics simulation (Table S1); N2 adsorption analysis (Table S2); reproducibility analysis (Figure S2); TEM and HRSTEM characterization of SBA-15, unsupported Ag NCs, and Ag NCs/S...

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Autores: Manno, Roberta, Ranjan, Prabhat, Sebastián, Víctor, Mallada, Reyes, Irusta, Silvia, Sharma, Upendra K., Eycken, Erik V. van der, Santamaría, Jesús
Tipo de recurso: conjunto de datos
Fecha de publicación:2020
País:España
Institución:Consejo Superior de Investigaciones Científicas (CSIC)
Repositorio:DIGITAL.CSIC. Repositorio Institucional del CSIC
OAI Identifier:oai:digital.csic.es:10261/362274
Acceso en línea:http://hdl.handle.net/10261/362274
Access Level:acceso abierto
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spelling Supporting Information: Continuous microwave-assisted synthesis of silver nanoclusters confined in mesoporous SBA-15: Application in alkyne cyclizationsManno, RobertaRanjan, PrabhatSebastián, VíctorMallada, ReyesIrusta, SilviaSharma, Upendra K.Eycken, Erik V. van derSantamaría, JesúsOptimization of heating time in batch synthesis (Figure S1); physical and geometrical parameters adopted for Comsol Multiphysics simulation (Table S1); N2 adsorption analysis (Table S2); reproducibility analysis (Figure S2); TEM and HRSTEM characterization of SBA-15, unsupported Ag NCs, and Ag NCs/SBA-15 with 0.16, 0.62, and 0.96 wt % (Figure S3); leaching test for propargylguanidine cyclization (Figure S4, Table S3, and Figure S5); catalytic reusability and stability study by reaction of 2-(phenylethynyl)phenol (Figure S6); continuous flow reaction and activation energy for 2-(phenylethynyl)phenol cyclization (figure S7); reaction mechanism for hydroamination of propargylguanidines (Scheme S1); general procedure for the synthesis of starting material with corresponding characterization data.Peer reviewedAmerican Chemical SocietyConsejo Superior de Investigaciones Científicas [https://ror.org/02gfc7t72]202420242020info:eu-repo/semantics/datasethttp://purl.org/coar/resource_type/c_ddb1application/pdfhttp://hdl.handle.net/10261/362274reponame:DIGITAL.CSIC. Repositorio Institucional del CSICinstname:Consejo Superior de Investigaciones Científicas (CSIC)InglésManno, Roberta; Ranjan, Prabhat; Sebastián, Víctor; Mallada, Reyes; Irusta, Silvia; Sharma, Upendra K.; Eycken, Erik V. van der; Santamaría, Jesús. Continuous microwave-assisted synthesis of silver nanoclusters confined in mesoporous SBA-15: Application in alkyne cyclizations. https://doi.org/10.1021/acs.chemmater.9b04935. http://hdl.handle.net/10261/362266Síinfo:eu-repo/semantics/openAccessoai:digital.csic.es:10261/3622742026-05-22T06:33:51Z
dc.title.none.fl_str_mv Supporting Information: Continuous microwave-assisted synthesis of silver nanoclusters confined in mesoporous SBA-15: Application in alkyne cyclizations
title Supporting Information: Continuous microwave-assisted synthesis of silver nanoclusters confined in mesoporous SBA-15: Application in alkyne cyclizations
spellingShingle Supporting Information: Continuous microwave-assisted synthesis of silver nanoclusters confined in mesoporous SBA-15: Application in alkyne cyclizations
Manno, Roberta
title_short Supporting Information: Continuous microwave-assisted synthesis of silver nanoclusters confined in mesoporous SBA-15: Application in alkyne cyclizations
title_full Supporting Information: Continuous microwave-assisted synthesis of silver nanoclusters confined in mesoporous SBA-15: Application in alkyne cyclizations
title_fullStr Supporting Information: Continuous microwave-assisted synthesis of silver nanoclusters confined in mesoporous SBA-15: Application in alkyne cyclizations
title_full_unstemmed Supporting Information: Continuous microwave-assisted synthesis of silver nanoclusters confined in mesoporous SBA-15: Application in alkyne cyclizations
title_sort Supporting Information: Continuous microwave-assisted synthesis of silver nanoclusters confined in mesoporous SBA-15: Application in alkyne cyclizations
dc.creator.none.fl_str_mv Manno, Roberta
Ranjan, Prabhat
Sebastián, Víctor
Mallada, Reyes
Irusta, Silvia
Sharma, Upendra K.
Eycken, Erik V. van der
Santamaría, Jesús
author Manno, Roberta
author_facet Manno, Roberta
Ranjan, Prabhat
Sebastián, Víctor
Mallada, Reyes
Irusta, Silvia
Sharma, Upendra K.
Eycken, Erik V. van der
Santamaría, Jesús
author_role author
author2 Ranjan, Prabhat
Sebastián, Víctor
Mallada, Reyes
Irusta, Silvia
Sharma, Upendra K.
Eycken, Erik V. van der
Santamaría, Jesús
author2_role author
author
author
author
author
author
author
dc.contributor.none.fl_str_mv Consejo Superior de Investigaciones Científicas [https://ror.org/02gfc7t72]
description Optimization of heating time in batch synthesis (Figure S1); physical and geometrical parameters adopted for Comsol Multiphysics simulation (Table S1); N2 adsorption analysis (Table S2); reproducibility analysis (Figure S2); TEM and HRSTEM characterization of SBA-15, unsupported Ag NCs, and Ag NCs/SBA-15 with 0.16, 0.62, and 0.96 wt % (Figure S3); leaching test for propargylguanidine cyclization (Figure S4, Table S3, and Figure S5); catalytic reusability and stability study by reaction of 2-(phenylethynyl)phenol (Figure S6); continuous flow reaction and activation energy for 2-(phenylethynyl)phenol cyclization (figure S7); reaction mechanism for hydroamination of propargylguanidines (Scheme S1); general procedure for the synthesis of starting material with corresponding characterization data.
publishDate 2020
dc.date.none.fl_str_mv 2020
2024
2024
dc.type.none.fl_str_mv info:eu-repo/semantics/dataset
http://purl.org/coar/resource_type/c_ddb1
format dataset
dc.identifier.none.fl_str_mv http://hdl.handle.net/10261/362274
url http://hdl.handle.net/10261/362274
dc.language.none.fl_str_mv Inglés
language_invalid_str_mv Inglés
dc.relation.none.fl_str_mv Manno, Roberta; Ranjan, Prabhat; Sebastián, Víctor; Mallada, Reyes; Irusta, Silvia; Sharma, Upendra K.; Eycken, Erik V. van der; Santamaría, Jesús. Continuous microwave-assisted synthesis of silver nanoclusters confined in mesoporous SBA-15: Application in alkyne cyclizations. https://doi.org/10.1021/acs.chemmater.9b04935. http://hdl.handle.net/10261/362266
Sí
dc.rights.none.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
dc.publisher.none.fl_str_mv American Chemical Society
publisher.none.fl_str_mv American Chemical Society
dc.source.none.fl_str_mv reponame:DIGITAL.CSIC. Repositorio Institucional del CSIC
instname:Consejo Superior de Investigaciones Científicas (CSIC)
instname_str Consejo Superior de Investigaciones Científicas (CSIC)
reponame_str DIGITAL.CSIC. Repositorio Institucional del CSIC
collection DIGITAL.CSIC. Repositorio Institucional del CSIC
repository.name.fl_str_mv
repository.mail.fl_str_mv
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