Supporting Information: Continuous microwave-assisted synthesis of silver nanoclusters confined in mesoporous SBA-15: Application in alkyne cyclizations
Optimization of heating time in batch synthesis (Figure S1); physical and geometrical parameters adopted for Comsol Multiphysics simulation (Table S1); N2 adsorption analysis (Table S2); reproducibility analysis (Figure S2); TEM and HRSTEM characterization of SBA-15, unsupported Ag NCs, and Ag NCs/S...
| Autores: | , , , , , , , |
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| Tipo de recurso: | conjunto de datos |
| Fecha de publicación: | 2020 |
| País: | España |
| Institución: | Consejo Superior de Investigaciones Científicas (CSIC) |
| Repositorio: | DIGITAL.CSIC. Repositorio Institucional del CSIC |
| OAI Identifier: | oai:digital.csic.es:10261/362274 |
| Acceso en línea: | http://hdl.handle.net/10261/362274 |
| Access Level: | acceso abierto |
| Sumario: | Optimization of heating time in batch synthesis (Figure S1); physical and geometrical parameters adopted for Comsol Multiphysics simulation (Table S1); N2 adsorption analysis (Table S2); reproducibility analysis (Figure S2); TEM and HRSTEM characterization of SBA-15, unsupported Ag NCs, and Ag NCs/SBA-15 with 0.16, 0.62, and 0.96 wt % (Figure S3); leaching test for propargylguanidine cyclization (Figure S4, Table S3, and Figure S5); catalytic reusability and stability study by reaction of 2-(phenylethynyl)phenol (Figure S6); continuous flow reaction and activation energy for 2-(phenylethynyl)phenol cyclization (figure S7); reaction mechanism for hydroamination of propargylguanidines (Scheme S1); general procedure for the synthesis of starting material with corresponding characterization data. |
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