Solvent-resistant ultrafiltration to recover bioactive compounds from wet olive pomace extracts

[EN] To contribute to the circular economy in olive mills, wet olive pomace can be employed as a source of valuable phenolic compounds. These compounds are efficiently extracted with ethanol/water 50:50 (v/v), at 40 °C. Here, the ultrafiltration membranes UF010104, UF010801v3 (from SolSep BV), and U...

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Autores: Sánchez-Arévalo, Carmen María|||0000-0001-6357-8107, Iborra Clar, Alicia|||0000-0001-5937-8428, Vincent Vela, Maria Cinta|||0000-0001-8493-0165, Alvarez Blanco, Silvia
Tipo de recurso: artículo
Fecha de publicación:2023
País:España
Institución:Universitat Politècnica de València (UPV)
Repositorio:RiuNet. Repositorio Institucional de la Universitat Politécnica de Valéncia
Idioma:inglés
OAI Identifier:oai:riunet.upv.es:10251/205877
Acceso en línea:https://riunet.upv.es/handle/10251/205877
Access Level:acceso abierto
Palabra clave:Solvent-resistant ultrafiltration
Ultrafiltration
Ethanol
Phenolic compounds
Wet olive pomace
INGENIERIA QUIMICA
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repository_id_str
spelling Solvent-resistant ultrafiltration to recover bioactive compounds from wet olive pomace extractsSánchez-Arévalo, Carmen María|||0000-0001-6357-8107Iborra Clar, Alicia|||0000-0001-5937-8428Vincent Vela, Maria Cinta|||0000-0001-8493-0165Alvarez Blanco, SilviaSolvent-resistant ultrafiltrationUltrafiltrationEthanolPhenolic compoundsWet olive pomaceINGENIERIA QUIMICA[EN] To contribute to the circular economy in olive mills, wet olive pomace can be employed as a source of valuable phenolic compounds. These compounds are efficiently extracted with ethanol/water 50:50 (v/v), at 40 °C. Here, the ultrafiltration membranes UF010104, UF010801v3 (from SolSep BV), and UP005 (Microdyn Nadir) have been tested to purify the phenolic compounds present in the hydroalcoholic extracts of the pomace. Several membrane conditioning protocols were explored, being the most adequate a short pre-treatment consisting of soaking the membrane in the working solvent for 2 h. All the considered membranes permitted the recovery of the biophenols of interest in the permeate stream, being most of the organic matter retained. A powerful analytical methodology based on liquid chromatography coupled to mass spectrometry (LC-ESI-QToF-MS) allowed the evaluation of the individual rejection of 43 compounds. The UF010104 membrane displayed the highest permeate flux (15 L h¿1·m¿2, at 2.5 bar) and high rejection of the total solids (67 ± 3%, at 2.5 bar), thus achieving the purification of the phenolic compounds in the permeate stream. The cleaning of the membranes used in organic solvent media was also investigated.This work was supported by MCIN/AEI/10.13039/501100011033 and by ERDF A way of making Europe, grant number CTM2017-88645-R. The predoctoral grant PRE2018-08524 was funded by MCIN/AEI/10.13039/501100011033 and by ESF Investing in your future. Funding for open access charge: CRUE-Universitat Politecnica de Valencia.ElsevierDepartamento de Ingeniería Química y NuclearEscuela Técnica Superior de Ingeniería IndustrialInstituto Universitario de Seguridad Industrial, Radiofísica y MedioambientalEuropean Social FundAGENCIA ESTATAL DE INVESTIGACIONEuropean Regional Development FundUniversitat Politècnica de ValènciaRepositorio Institucional de la Universitat Politècnica de València Riunet20232023-08-15journal articlehttp://purl.org/coar/resource_type/c_6501VoRhttp://purl.org/coar/version/c_970fb48d4fbd8a85info:eu-repo/semantics/articleapplication/pdfhttps://riunet.upv.es/handle/10251/205877reponame:RiuNet. Repositorio Institucional de la Universitat Politécnica de Valénciainstname:Universitat Politècnica de València (UPV)InglésengAgencia Estatal de Investigación http://dx.doi.org/10.13039/501100011033 Plan Estatal de Investigación Científica y Técnica y de Innovación 2013-2016 CTM2017-88645-R IMPLEMENTACION DE TECNOLOGIA DE MEMBRANAS PARA LA VALORIZACION DE LOS COMPUESTOS FENOLICOS PRESENTES EN LAS AGUAS RESIDUALES DE LA INDUSTRIA DE PRODUCCION DE ACEITE DE OLIVAAgencia Estatal de Investigación http://dx.doi.org/10.13039/501100011033 PRE2018-085245 AYUDA PARA CONTRATOS PREDOCTORALES PARA LA FORMACION DE DOCTORES-SANCHEZ AREVALO, CARMEN. PROYECTO: IMPLEMENTACION DE TECNOLOGIA DE MEMBRANAS PARA LA VALORIZACION DE LOS COMPUESTOS FENOLICOS PRESENTES EN LAS AGUAS RESIDUALESopen accesshttp://purl.org/coar/access_right/c_abf2Reconocimiento - No comercial - Sin obra derivada (by-nc-nd) http://creativecommons.org/licenses/by-nc-nd/4.0/info:eu-repo/semantics/openAccessoai:riunet.upv.es:10251/2058772026-06-13T07:49:27Z
dc.title.none.fl_str_mv Solvent-resistant ultrafiltration to recover bioactive compounds from wet olive pomace extracts
title Solvent-resistant ultrafiltration to recover bioactive compounds from wet olive pomace extracts
spellingShingle Solvent-resistant ultrafiltration to recover bioactive compounds from wet olive pomace extracts
Sánchez-Arévalo, Carmen María|||0000-0001-6357-8107
Solvent-resistant ultrafiltration
Ultrafiltration
Ethanol
Phenolic compounds
Wet olive pomace
INGENIERIA QUIMICA
title_short Solvent-resistant ultrafiltration to recover bioactive compounds from wet olive pomace extracts
title_full Solvent-resistant ultrafiltration to recover bioactive compounds from wet olive pomace extracts
title_fullStr Solvent-resistant ultrafiltration to recover bioactive compounds from wet olive pomace extracts
title_full_unstemmed Solvent-resistant ultrafiltration to recover bioactive compounds from wet olive pomace extracts
title_sort Solvent-resistant ultrafiltration to recover bioactive compounds from wet olive pomace extracts
dc.creator.none.fl_str_mv Sánchez-Arévalo, Carmen María|||0000-0001-6357-8107
Iborra Clar, Alicia|||0000-0001-5937-8428
Vincent Vela, Maria Cinta|||0000-0001-8493-0165
Alvarez Blanco, Silvia
author Sánchez-Arévalo, Carmen María|||0000-0001-6357-8107
author_facet Sánchez-Arévalo, Carmen María|||0000-0001-6357-8107
Iborra Clar, Alicia|||0000-0001-5937-8428
Vincent Vela, Maria Cinta|||0000-0001-8493-0165
Alvarez Blanco, Silvia
author_role author
author2 Iborra Clar, Alicia|||0000-0001-5937-8428
Vincent Vela, Maria Cinta|||0000-0001-8493-0165
Alvarez Blanco, Silvia
author2_role author
author
author
dc.contributor.none.fl_str_mv Departamento de Ingeniería Química y Nuclear
Escuela Técnica Superior de Ingeniería Industrial
Instituto Universitario de Seguridad Industrial, Radiofísica y Medioambiental
European Social Fund
AGENCIA ESTATAL DE INVESTIGACION
European Regional Development Fund
Universitat Politècnica de València
Repositorio Institucional de la Universitat Politècnica de València Riunet
dc.subject.none.fl_str_mv Solvent-resistant ultrafiltration
Ultrafiltration
Ethanol
Phenolic compounds
Wet olive pomace
INGENIERIA QUIMICA
topic Solvent-resistant ultrafiltration
Ultrafiltration
Ethanol
Phenolic compounds
Wet olive pomace
INGENIERIA QUIMICA
description [EN] To contribute to the circular economy in olive mills, wet olive pomace can be employed as a source of valuable phenolic compounds. These compounds are efficiently extracted with ethanol/water 50:50 (v/v), at 40 °C. Here, the ultrafiltration membranes UF010104, UF010801v3 (from SolSep BV), and UP005 (Microdyn Nadir) have been tested to purify the phenolic compounds present in the hydroalcoholic extracts of the pomace. Several membrane conditioning protocols were explored, being the most adequate a short pre-treatment consisting of soaking the membrane in the working solvent for 2 h. All the considered membranes permitted the recovery of the biophenols of interest in the permeate stream, being most of the organic matter retained. A powerful analytical methodology based on liquid chromatography coupled to mass spectrometry (LC-ESI-QToF-MS) allowed the evaluation of the individual rejection of 43 compounds. The UF010104 membrane displayed the highest permeate flux (15 L h¿1·m¿2, at 2.5 bar) and high rejection of the total solids (67 ± 3%, at 2.5 bar), thus achieving the purification of the phenolic compounds in the permeate stream. The cleaning of the membranes used in organic solvent media was also investigated.
publishDate 2023
dc.date.none.fl_str_mv 2023
2023-08-15
dc.type.none.fl_str_mv journal article
http://purl.org/coar/resource_type/c_6501
VoR
http://purl.org/coar/version/c_970fb48d4fbd8a85
dc.type.openaire.fl_str_mv info:eu-repo/semantics/article
format article
dc.identifier.none.fl_str_mv https://riunet.upv.es/handle/10251/205877
url https://riunet.upv.es/handle/10251/205877
dc.language.none.fl_str_mv Inglés
eng
language_invalid_str_mv Inglés
language eng
dc.relation.none.fl_str_mv Agencia Estatal de Investigación http://dx.doi.org/10.13039/501100011033 Plan Estatal de Investigación Científica y Técnica y de Innovación 2013-2016 CTM2017-88645-R IMPLEMENTACION DE TECNOLOGIA DE MEMBRANAS PARA LA VALORIZACION DE LOS COMPUESTOS FENOLICOS PRESENTES EN LAS AGUAS RESIDUALES DE LA INDUSTRIA DE PRODUCCION DE ACEITE DE OLIVA
Agencia Estatal de Investigación http://dx.doi.org/10.13039/501100011033 PRE2018-085245 AYUDA PARA CONTRATOS PREDOCTORALES PARA LA FORMACION DE DOCTORES-SANCHEZ AREVALO, CARMEN. PROYECTO: IMPLEMENTACION DE TECNOLOGIA DE MEMBRANAS PARA LA VALORIZACION DE LOS COMPUESTOS FENOLICOS PRESENTES EN LAS AGUAS RESIDUALES
dc.rights.none.fl_str_mv open access
http://purl.org/coar/access_right/c_abf2
Reconocimiento - No comercial - Sin obra derivada (by-nc-nd)
http://creativecommons.org/licenses/by-nc-nd/4.0/
dc.rights.openaire.fl_str_mv info:eu-repo/semantics/openAccess
rights_invalid_str_mv open access
http://purl.org/coar/access_right/c_abf2
Reconocimiento - No comercial - Sin obra derivada (by-nc-nd)
http://creativecommons.org/licenses/by-nc-nd/4.0/
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
dc.publisher.none.fl_str_mv Elsevier
publisher.none.fl_str_mv Elsevier
dc.source.none.fl_str_mv reponame:RiuNet. Repositorio Institucional de la Universitat Politécnica de Valéncia
instname:Universitat Politècnica de València (UPV)
instname_str Universitat Politècnica de València (UPV)
reponame_str RiuNet. Repositorio Institucional de la Universitat Politécnica de Valéncia
collection RiuNet. Repositorio Institucional de la Universitat Politécnica de Valéncia
repository.name.fl_str_mv
repository.mail.fl_str_mv
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score 15,81155

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