Ni-Ru supported on CeO2 obtained by mechanochemical milling for catalytic hydrogen production from ammonia

Developing active and stable catalysts for carbon-free hydrogen production is crucial to mitigate the effects of climate change. Ammonia is a promising carbon-free hydrogen source, as it has a high hydrogen content and is liquid at low pressure, which allows its easy storage and transportation. We h...

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Detalles Bibliográficos
Autores: Lucentini, Ilaria, Serrano, Isabel, Garcia, Xènia, Garzón Manjón, Alba, Hu, Xinxin, Arbiol, Jordi, Pascua-Solé, Laia, Prat, Jordi, Villalobos-Portillo, Edgar Eduardo, Marini, Carlo, Escudero, Carlos, Llorca, Jordi
Tipo de recurso: artículo
Estado:Versión publicada
Fecha de publicación:2024
País:España
Institución:Consejo Superior de Investigaciones Científicas (CSIC)
Repositorio:DIGITAL.CSIC. Repositorio Institucional del CSIC
OAI Identifier:oai:digital.csic.es:10261/376146
Acceso en línea:http://hdl.handle.net/10261/376146
Access Level:acceso abierto
Palabra clave:http://metadata.un.org/sdg/13
Take urgent action to combat climate change and its impacts
Descripción
Sumario:Developing active and stable catalysts for carbon-free hydrogen production is crucial to mitigate the effects of climate change. Ammonia is a promising carbon-free hydrogen source, as it has a high hydrogen content and is liquid at low pressure, which allows its easy storage and transportation. We have recently developed a nickel-based catalyst with a small content of ruthenium supported on cerium oxide, which exhibits high activity and stability in ammonia decomposition. Here, we investigate mechanochemical milling for its synthesis, a faster and less energy-consuming technique than conventional ones. Results indicate that mechanochemical synthesis increases catalytic activity compared to the conventional incipient wetness impregnation method. The interaction between the metal precursors and the support is key in fine-tuning catalytic activity, which increases linearly with oxygen vacancies in the support. Moreover, the mechanochemical method modifies the oxidation state of Ni and Ru species, with a variation depending on the precursors.