Bifunctional Aminotriphenolate Complexes as One-Component Catalysts for the ROCOP of Cyclic Anhydrides and Epoxides

Bifunctional aminotriphenolate complexes derived from trivalent metals (M = Co, Mn, Cr) have been prepared and structurally characterized. These complexes are octahedral in the solid state but infer dynamic behavior of the ligated dimethylaminopyridine (DMAP) ligands that can function as initiators...

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Detalles Bibliográficos
Autores: Martín, Carmen, Pizzolante, Antonella, Escudero-Adán, Eduardo C., Kleij, Arjan W.
Tipo de recurso: artículo
Estado:Versión aceptada para publicación
Fecha de publicación:2018
País:España
Institución:Varias* (Consorci de Biblioteques Universitáries de Catalunya, Centre de Serveis Científics i Acadèmics de Catalunya)
Repositorio:Recercat. Dipósit de la Recerca de Catalunya
OAI Identifier:oai:recercat.cat:2072/356186
Acceso en línea:http://hdl.handle.net/2072/356186
https://doi.org/10.1002/ejic.201800142
Access Level:acceso abierto
Palabra clave:54
Descripción
Sumario:Bifunctional aminotriphenolate complexes derived from trivalent metals (M = Co, Mn, Cr) have been prepared and structurally characterized. These complexes are octahedral in the solid state but infer dynamic behavior of the ligated dimethylaminopyridine (DMAP) ligands that can function as initiators in the ring-opening copolymerization of cyclic anhydrides and epoxides. More specifically, the ring-opening copolymerization of cyclohexene oxide and phthalic anhydride was studied in detail, and the bifunctional Cr(III) complex gave overall the best results in terms of overall activity and polyester quality.